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GCMS analysis results for sample AE08067, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting the GCMS analysis of sample AE08067 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046799–000046812

Folder label: “GCMS X 4/5/02 A 4/16/02

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Scanned page image, NYC-WTC_000046809
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020415\08067.D Vial: 24 Acq On 16 Apr 2002 5:36 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.02 0.80 ug/L 446960 1,4-Dichlorobenzene-d4 9.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

- 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 83 2 Butane, 2,2,3,3 - tetranitro- 238 C4H6N4O8 020919-97-5 12 3 Hexyl octyl ether 214 C14H30O 017071-54-4 9 4 2-Propanone, 1,1-dichloro-_________ 126 C3H4C120 000513-88-2 9 Abundance Scan 500 (6 017 min) 08067 D (-495) (-) m/z 43.30 100.00% 43 A 5000

125 5 60 5 80 6 00 6.20 6.40 01 ---PPPPP 35 , 63 97 + > I I'l'l , 11 । । > , I IM > | I I 11 83 117 I, m/z 125.20 10.88% Tl/Z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #3877 2-Propanone, 1.1.1-tri chloro- 43

5000 . ...... A....... 560 5.80 600 6 20 6 40 m/z 97.20 6.92% 15 27 36 . ,50 63 76 8!3 8 9 97. 110 117 125 0— TP 11——mtutmTBOmHIPTTT Tl/Z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #3995: Butane, 2,2,3.3-tetranitro- 30 43 ____60__________ 5 5.80 600 6.20 640 5000 m/z 47.20 6.08% 53 15

n/z— > 01 jillposi 10 20 —30 +4 1’ 'IiliI h। ■ i । । 69। ■ 40 86 50 60 70 80 90 100 110 120 130 140 150 Abundance #7098 Hexyl octyl ether 43 57 85 5.60 5 80 6.00 6 20 6.40 71 m/z 83.20 5.98% 5000

29

n/z- > 0 - 44 10 20 30 40 50 ++ 1.97103 1...........143 60 70) 80 112 r' I 1 1 ' ' I ' ' ' ' I 1 1 ' ' 1 1 ' ' 1 1 1 1 1 ' 1 1 1 ' 1 I ' 90 100 110 120 130 140 150 5.60 5.80 6.00 6.20 6.40

08067.D 041202SCAN.M Tue Apr 16 13:56:08 2002 Page 7

NYC-WTC_000046809

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NYC-WTC_000046809Source: NYC Law Department, mirrored locally

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