GCMS results for sample AE08068, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On 16 Apr 2002 6:25 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 12 2-Propanone, 1,1,1-trichloro- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 6.02 0.74 ug/L 486692 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 50 2 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 3 1-Fluorononane 146 C9H19F 000463-18-3 9 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 7 Abundance Scan 501 (6 023 min) 08068 D (-496) (-) m/z 43.30 100.00% 43

5000

1 5 60 5 80 6 00 6 20 6 40

n/z-> Ol ......... 85,7 . i?1 83 82. 97 117 127 1 ■' i ' 1 1 ■ i11 ■ ■ । 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 । । nr. । ‘ । ‘ I . . .. ।। . ।. 1’ ।।। . m/z 125.20 10.15% Abundance #3877: 2-Propanone, 1,1,1-trichloro- 43

5000 1 5 60 5 80 1 6.00 6.20 6 40 m/z 97.10 7.16% 15 07 I 27 36 ,50 63 7 6 83 97 110117 125 01 TIIT 1 ■ rl ■ ■ ■ ■ r1'' ■ ■ । ' 1' ।1 । ■' । ■ ' ''''I'' '' । ■ ' । ■ ' । ■ . ■ ■ । ■ . ■. ।. n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #3861 2-Propanone, 1,1-di chloro- 43

5 60 5.80 6 00 6 20 6.40 5000 m/z 127.10 6.39%

15 27 I I 36 1 ,,|'l ■ ■ ■ ■ 11 '' ■ i ■ ■ 1 ' i ’ Ol TLTPNT 50 63 76 83 93 125 ■ !'■ ' ■ ■ । ■ > ■ ■ । ■ ■ ■ ’ । ■ ■ • ■ । । । । । ■ Tl/Z—> Abundance 10 20 30 40

43 50 60 70 80 #4248 1-Fluorononane 90 100 110 120 130 140 150

5.60 5 80 J..... 6.00 6.20 6.40 m/z 47.20 6.16% 55 | 5000 29

15 0 '' I ' ' '' I ' +36. +4 +24+ +Z71L 70 84 97

| 104 111 118 126 146 it ■ 1111 ' ■ ■ i - 1 1 ■ ।■■ ■. । • ' ■ ■ । ■ > ■■ ।. wMMAAbphmpy । ' ■ 1 ' i ■ r 1 ' । 1 1 1 1 iB| 1 ,-n 1 11 /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 5 60 580 600 6.20 6.40

08068.D 041202SCAN.M Tue Apr 16 13:56:52 2002 Page 15

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