GCMS results for sample AE08068, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On 16 Apr 2002 6:25 am Operator: Nefliu Sample sample Inst : Instrumen Misc : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 N-Ethylformamide Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T. 5.96 0.34 ug/L 223036 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide C3H7NO 73 000627-45-2 9 2 2-Hydroxy-2-methylbutanoic acid C5H10O3 118 1000196-27-1 9 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H1404 1000186-02-3 9 4 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 7 Abundance Scan 491 (5.964 min) 08068 D (-485) (-) m/z 73.30 100.00% 73

5000 43

1 I 55 86 103 5 60 5 80 6 00 6 20 6.40

n/z--> O' ' r mi i " " i' " ' i mmmWIPPmmmTTTT ii 1111'11' 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 43.25 30.28% Abundance #857 N-Ethylformamide 3b 73

5000 44 58 _AM 5 60 5.80 6.00 6.20 6.40 m/z 45.20 9.46% 18 0 111 nr i14 —p r " ‘ 11 ■' i ■11■i■■■■i'■■■i■' " i " 1' i'1111 1111111111' ।1111111111 n/z— > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25613 2-Hydroxy-2-methylbutanoic acid 73

5 60 5 80 6 00 6.20 6.40 5000 43 55 m/z 41.30 9.38%

29

n/z— > 0- 10 20 l H—— + 30 40 .... ...... . ........ ...... ........ 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344' Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 1 ‘Inna i 113 "I7 73 5 60 5 80 6.00 6 20 640 m/ z 71.30 6.51% | 5000

43

Tl/Z—> 0 27 1' I ''1' I ' - ' I ■ ■ '1 r ''' T' 10 20 30 40 50 55 60 70 | 80 87 113 131 90 100 110 120 130 140 150 160 170 180 174 5.60 5.80 1.1.... 6 00 6 20 640

08068.D 041202SCAN.M Tue Apr 16 13:56:52 2002 Page 14

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