GCMS analysis results for sample AE08428, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020419\08428.D Vial : 15 Acq On 19 Apr 2002 9:55 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title Method 508 GC/MS Scan Library C:\DATABASE\nist98.1 Peak Number 2 N-Ethylformamide Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.11 0.27 ug/1 399027 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual l N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1-Propene-l-thiol 74 C3H6S 000925-89-3 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 9 Abundance Scan 515 (6.105 min): 08428. D (-507) (-) m/z 73.10 100.00% 73

5000 43 । । । । । । । ri । । । । PPPt [....... 87 103 5.80 6.00 6.20 6.40 , 38 1)1 50 55...... , I r' I ' ' ' ■ I • - 1 ’I"1 . . I I I . , I I I Trl >■! I I I I m/ z 43.10 31.10% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #857: N-Ethylformamide 30 73

5000 wpMnnkwudt ,, “MWh 58 5.80 6.00 6.20 6.40 44 m/z 41.10 ( 12.20% 18 —134—25 m/z->______ 10 20 nr. .w.,.. 30 40 50 — ———————————— ———————— 60 70 80 90 100 110 Abundance #25348:1-Propene-1 -thiol 73 5.80 6.00 6.20 6.40 5000 m/z 45.10 8.14%

n/z-> Abundance

5000 38, , 49 55 60 67 , |, — ——————— 10 —— 20 30 40 43

50 60 70 #25472: Pentane, 3-methoxy- 80

73 90 100 110 11.1,1...... m/z 5.80 6.00 71.10 w 6.20 —1 6.40 5.84%

45

m/z-> —... 7.. > 10 20 30 40 50 55 T1—PPP 4PI 50 60 70 80 67 ' i ' 1 90 1 101 ■ i ' ' ■ ■ i 1 100 110 R...... ............. ' ■ i ‘ 1 1 1 i ■ ■ 1 1 I"T 1 1 1 1 1 1 1 5.80 6.00 6.20 6.40

08428.D SCAN020418.M Thu May 02 15:36:03 2002 Page 4

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