GCMS analysis results for sample AE08428, May 2002

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Library Search Compound Report

Data File : C : \MSDCHEM\ 1 \DATA\020419\08428.D Vial: 15 Acq On : 19 Apr 2002 9:55 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Heptane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.14 0.26 ug/1 385014 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 91 2 Heptane 100 C7H16 000142-82-5 83 3 Heptane 100 C7H16 000142-82-5 72 4 Hexane, 3-methyl-_________________ 100 C7H16 000589-34-4 53 Abundance Scan 11 (3.144 min): 08428.D (-5) (-) m/z 43.15 100.00% 43 71 5000 57

100

meUrni +4— 86 3.20 3.30 3.40 3.50 3.60 36 | ' ' I ' ' ' I I I I I I I 1 1 1 1 I ri l । । । > । |-v ‘T m/z 71.10 54.32% n/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #109668: Heptane 43

5000 57 71 w. PTYPPP—PT 3.20 3.30 3.40 3.50 3.60 29 m/ z 41.10 47.67% — 100

n/z-> 0 । 1 1 ■ ' i ■ 10 ,1 22.1, 20 , , ,371 1 1 1 11 1 1 1 1 1 1 1 30 40 +5114 50 tTT +477,85,91...... (60 63 70 80 90 100 Abundance #109598: Heptane 43 3.20 3.30 3.40 3.50 3.60 5000 57 m/z 57.15 45.19% 29 71

/ +514 85 190 m/z-> ............... 0 10 20 1 1137, 30 40 50 . 63 1 I ' ' ' ' I'1 T—BD-—T 60 70 80 90 100 Abundance #4133: Heptane -44444 43 3.20 3.30 3.40 3.50 3.60 m/z 56.10 29.20% 5000 29 57 71

15 100 2 , 51, | 85 ■ ■ i ■ ■ > ■ i ■ 4 -P +4. 1 IT t65 mmmmmmme । । MAMI 1,4818,1/ P । । tJz-> 0 10 20 30 40 50 (60 70 80 90 100 3.20 3.30 3.40 3.50 3.60

08428.D SCAN020418 .M Thu May 02 15:36:01 2002 Page 3

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