GCMS analysis results for sample AE08324, May 2002

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Data File : C:\MSDCHEM\1\DATA\020419\08324.D Vial: 11 Acq On : 19 Apr 2002 5:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Heptane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

3.14 0.31 ug/1 439218 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 64 2 Hexane, 3-methyl- 100 C7H16 000589-34-4 53 3 Hexane, 3-methyl- 100 C7H16 000589-34-4 53 4 Heptane 100 C7H16 000142-82-5 47 Abundance Scan 10 (3.138 min): 08324.D (-3) (-) m/ z 43.15 100.00% 40

5000 57 71

100 ' 1 I 1 ' ' ' I 1 1 1 1 । 1 1 1' ।1 ■r ■ ।' 3.20 3.30 3.40 3.50 3.60

Tl/Z--> 1 I I 'I

0 I f f I

10 I I I I [ “I_ I

20 I I I

30 1 35 ill 440 5051 1 60 ' ' 1 1 1 ■ i ■ ■ — —Iy

70 80 i 85 i r i ,

90 i f i i

100 T TIT m/ z 71.10 49.31%

Abundance #4133: Heptane 43

5000 29 57 71 --TPPP 3.20 3.30 3.40 3.50 3.60 m/z 57.15 45.91% 100 15 2 — , 51, | ,__ 65 85 m/z—> 1 1 । 1 1 1 1 1 1- 30 40 ‘1 T 1' 1 1 1 1 1 11‛ni l ' 1 । ' ' । ‘II 0 10 20 50 I60 70 80 90 100 Abundance #5587: Hexane, 3-methyl- 40 fif 3.20 3.30 3.40 3.50 3.60 5000 57 m/z 40.10 36.02% 71 29

n/z-> --21 o 10 20 13611 +5114 65 — — : 50 I60 70 78 85 ———— 80 90 100 100 30 40 1 I ' 1 1

Abundance #109291: Hexane, 3-methyl- 1 ' ' ' i 1 ■ ■ ■ i ■ ‘ 1 1 i 1 ' ' 1 i 1 ’ ' ■ i ■ 40 3.20 3.30 3.40 3.50 3.60 m/z 41.10 34.72%

5000 57 71

m/z-> ................................ I | ' ' I ‘ 1 1 1 1 1 1 1 ' 1 1 1 ' < ( 1 1 1 I [I 0 10 20 30 40 +514 50 65 85 ' i 1 ' 1 ’ l 1 > > > । ■ i' > > । < ■ ■ ■ | ■ ■ - > । 60 70 80 90 100 100 3.20 3.30 3.40 3.50 3.60

08324 .D SCAN020418.M Fri May 03 09:04:31 2002 Page 3

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