GCMS analysis results for sample AE08426, May 2002

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Data File C:\MSDCHEM\l\DATA\020419\08426.D Vial: 13 Acq On 19 Apr 2002 7:57 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Heptane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.14 0.21 ug/1 296069 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 47 2 Heptane 100 C7H16 000142-82-5 45 3 Hexane, 3-methyl- 100 C7H16 000589-34-4 42 4 Hexane, 3-methyl- 100 C7H16 000589-34-4 40 Abundance Scan 10 (3.138 min): 08426.D (-3) (-) m/ z 43.15 100.00% 40

5000 57 71 — 100 86 । 3.20 3.30 3.40 3.50 3.60

m/z-> ................ 351, -Fr) ,i, i 0 10 20 30 40 50 , , 50 60 70 ----- 80 90 100 m/ z 41.15 39.87% Abundance #4133: Heptane 40

5000 29 57 71 3.20 3.30 3.40 3.50 3.60 m/z 57.05 39.18% 15 100

T87 2 - — ,1 । 1151.1 4’11 —65 ‘ । 1 1 । 1 85111 । I 1 ■ 1 । |' । TTT m/z-> 10 20 30 40 50 (60 70 80 90 100 Abundance #109598: Heptane 40

3.20 3.30 3.40 3 50 3.60 5000 57 m/z 71.10 30.71% 29 71

100

m/z—> i ■ 1 1 ' । 0 10 ‘ 20 । ' i1!, 1! । 137 30 1111 40 +51 50 TT 60 63 70 -PT 80 85 90 100 TT

Abundance #109291: Hexane, 3-methyl- 40 3.20 3.30 3.40 3.50 3.60 m/z 56.10 22.73% 5000 57 71

’IB +51 ' | 1 ' ' । I'i ........................... i '' 1 ' ' ' i 1 ' 1 i I, | ' i ■ ■ 65 ■ ■ ■ 85 100 pr । i'i । I । i । । | । । । । । , N /.A,M A.. m/z—> 0 10 20 30 40 50 60 70 80 90 100 3.20 3.30 3.40 3.50 3.60

08426.D SCAN020418.M Thu May 02 15:30:20 2002 Page 3

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