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GCMS analysis results for sample AE08426, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048169–000048181

Folder label: “GCMS X 4/9/02 A 4/19/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08426.D Vial: 13 Acq On : 19 Apr 2002 7:57 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 3-Buten-2-ol, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 5.01 0.69 ug/1 956489 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 81 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 64 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 50 4 1-Hexene, 4,5-dimethyl- 112 C8H16 016106-59-5 42 Abundance Scan 329 (5.012 min): 08426.D (-319) (-) m/ z 43.10 100.00% 43 71

....... ...................................... 5000 55 59 40

67 84 4.60 4.80 5.00 5.20 5.40 TTrruum i1111 r11111'111111'' ।111 I, lull,,,TTTH+ +75... 488..... m/z 71.10 91.49% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #114555: 3-Buten-2-ol, 2-methyl- 43 7h

5000 —PPR* 59 4.60 4.80 5.00 5.20 5.40 27 31 39 m/z 41.10 72.12% 53

n/z-> 5 1518 -... ili..... . 1+ +501561,-HH 67 HT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 86 TTPT Abundance #114557: 3-Buten-2-ol, 2-methyl- 43 7h 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 45.55% 59

27 31 39 53

m/z-> -H4 Tter E53= 67 86 ........ ... +i.......... Hrr....... l" 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #114556: 3-Buten-2-ol, 2-methyl- —9017 71 4.60 4.80 5.00 5.20 5.40 43 m/ z 55.00 39.01%

n/z—> 5000

5 50 -H 44 HH 156163,67 27 31 39 53

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 59

,74 86 M11" " i" " r1'1111" " i >1 -4-444444 WPhmspo 4.60 4.80 L 5.00 5.20 5.40

08426.D SCAN020418.M Thu May 02 15:30:21 2002 Page 4

NYC-WTC_000048176

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