GCMS results sample AE08255, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08255.D Vial: 13 Acq On 17 Apr 2002 7:22 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 3 3-Buten-2-ol, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

4.99 0.46 ug/L 491000 1,4-Dichlorobenzene-d4 9.99

Hit# of 5. Tentative ID MW MolForm CAS# Qual 1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 80 2 Butenol, methyl- 86 C5H10O 060766-00-9 56 3 Butanoic acid, 2-propenyl ester 128 C7H1202 002051-78-7 43 4 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 40 Abundance Scan 325 (4 989 min)' 08255.D (-320) (-) m/z 43.10 100.00% 43 71 4

5000 59

53 ■ ' । ■ ■1 1 i ■ '

n/z-> Abundance Ol ——mmT 10 20 30 40 ,1r I I... ”..... ......... rr 50 60 70 80 #114555: 3-Buten-2-ol, 2-methyl- 90 100 110 120 130 4 60 m/z 4.80 71.10 5 00 5.20 98.96% 5.40

43 7h

5000 59 4.60 All 4 80 5 00 5 20 5.40 27 m/ z 41.05 68.26% 53 01 - 18 l +44 86

n/z--> Abundance

5000 10 20

27 30 40

43 50 60

59 70I 80 #24435: Butenol, methyl- 7h 90 100 110 120 130

460 m/z 4 80 69.10 L 5 00 5 20 49.22% 5.40

15 53

Tl/Z-> 37 । Ol । PrH HP +—— 11, 10 20 30 40 50 60 +6544 .................................................... ... 70I 80 90 100 110 120 130 Abundance #6318: Butanoic acid, 2-propenyl ester ............ ........ - 43 71 4 60 4 80 5 00 5 20 5.40 m/ z 59.10 40.50%

5000 27

57

n/z-> 0 11135,01110711371 I1, । । ptl 1 rr rh 10 20 30 40 50 60 1———P-0—3—9———Pn—BBBUITr 70l , 82 89 80 90 100 113 128 100 110 120 130 4 60 4 80 5 00 * 5.20 h 5.40 0

08255.D 041702SCAN.M Thu Apr 18 09:24:57 2002 Page 7

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