GCMS results sample AE08255, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020417\08255.D Vial: 13 Acq On 17 Apr 2002 7:22 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 2 Toluene Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 4.39 7.77 ug/L 8244030 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3 94 2 Toluene 92 C7H8 000108-88-3 91 3 Toluene 92 C7H8 000108-88-3 91 4 Toluene 92 C7H8 000108-88-3 90 Abundance Scan 224 (4 395 min) 08255.D (-217) (-) m/ z 91.10 100.00% 91

5000

39 _ 51 55 4 00 4 20 4.40 4 60 4.80 1 45 " 60,i 74 86 0 ■ ■ । 1 ■ m/z 92.10 61.32% Tl/Z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117292 Toluene 91

5000 4.00 4 20 4 40 4.60 4.80 m/z 65.10 11.96% 39 51 65 27 .1 45 ? 57 1 | 77 86 ,, 01 IITPPPP 1........ n/z- > 0 10 20 30 40 50 60 70 80 90 100 Abundance #117281 Toluene 91

4 00 4 20 4 40 4.60 4 80 5000 m/z 39.10 9.46%

39 27 45 51 65 n/z-> 0- 1 ■ ■ T1 0 i ' 10 15 ' ■ ■ i 20 --- 30 40 50 37 „1,.56, 60 ... 70 1.,8086,1, 90 i 100 Abundance #117282: Toluene 91 4 00 4.20 4.40 4 60 4.80 m/z 63.10 7.67%

5000

n/z-> 0 1* । * ‘

0 10 20 27 30 39 . 51 65 .1 |111145l-|-1,l f * । "i - r [ * I.l i I < 1 । । ri'i 40 50 60 70 80 77 । । ri 86,, 90 1| 1 ■ 1 ■

100 i 1 ■ ......11....... 4 00 4 20 4.40 4.60 4 80

08255.D 041702SCAN.M Thu Apr 18 09:24:57 2002 Page 6

NYC-WTC_000047876