GCMS analysis results, Sample AE08262, April 22, 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020417\08262.D Vial: 19 Acq On : 18 Apr 2002 12:18 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Toluene Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 4.37 46.25 ug/L 45263000 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3 95 2 Toluene 92 C7H8 000108-88-3 94 3 Toluene 92 C7H8 000108-88-3 91 4 Toluene 92 C7H8 000108-88-3 90 Abundance Scan 219 (4 366 min): 08262 D (-212) (-) m/z 91.05 100.00% 91

5000

39 _ 51 65 4.00 4.20 4.40 4.60 4.80 01 10**** |J i ' 1 1 'i .I 45 .1 60,1 I 1 1 ‘l । i ' 74 ■' । 1 । 86 1 • I m/z 92.10 61.51% Tl/Z--> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117292: Toluene 91

5000 4.00 4 20 4.40 4 60 4 80 m/z 65.10 11.96% 39 51 65

n/z- > 0- 0 10 20 27 30 .1 40 45 2 50 60 57 ,| | 70 77— 80 864490 1

100 Abundance #117281: Toluene 9h

4 00 4.20 4 40 4.60 4.80 5000 m/z 39.10 9.39% 39 51 65 1 15 27 ...................................... .. 0- ' 11111' ।1'1111114 r1 n/z- > 0 10 20 30 40 50 60 70 80 90 100 Abundance #117282: Toluene 91 4 00 4 20 4.40 4.60 4 80 m/z 63.10 8.14% 5000

39 _ 51 65 27 45 51 | n/Z-> 0- 0 ------- 10 20 30 40 50 60 70 7 80—.,86,190 1

100 .... ........ ......... 4 00 4.20 4.40 4.60 4.80

08262.D 041702SCAN.M Thu Apr 18 09:49:31 2002 Page 10

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