GCMS results sample AE08258, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08258.D Vial: 16 Acq On : 17 Apr 2002 9:50 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 1 Toluene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 4.39 17.34 ug/L 18974900 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Toluene 92 C7H8 000108-88-3 95 2 Toluene 92 C7H8 000108-88-3 91 3 Toluene 92 C7H8 000108-88-3 91 4 Toluene 92 C7H8 000108-88-3 91 Abundance Scan 224 (4 395 min): 08258.D (-214) (-) m/z 91.10 100.00% 91

5000

39 , 51 65 4.00 4.20 4.40 4 60 4.80 I 45 II 61 | | 73 77 86 , 0- '•'I ""'I"" I'1 " . | 1 ' H I r i r i f l ur |I llrp-rn ,|I II ||I H 1,11! ||,! !| I, J)) ।11 ■" 111» m/ z 92.10 61.80% Tl/Z--> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #117292: Toluene 91

5000 4.00 4 20 4.40 4.60 4 80 m/z 65.10 11.62% 39 51 65

n/z-> 0— 15 ...25?7 ...... 20 1,1145.11771155, 30 35 40 45 50 61| 1 73 77 86 . " 111 ‘1.. ....... . " |..................... 1 —PP 55 60 65 70 75 80 85 90 95 100 Abundance #117282: Toluene 91

4.00 4 20 440 4 60 4 80 5000 m/z 39.10 9.26%

27 39 £ 51 65 0fT ' i11'' r ■ I 45 ? TTTTTt 61 I 73 77 86 ।111'111 " n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #37326: Toluene 91 4 00 4 20 4 40 4 60 4 80 m/ z 63.10 7.93% 5000

65 27 3 1 39 45 511 57 61 73 77 86 . 0— Tr......................... . 111 ■ ■ i ■ 11 ■ ■ ■ 11' 11' i " " i111111 ■ ■ ■ ।1'11 111 " 111111 " '11 —TT n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4 00 4.20 440 4.60 4.80

08258.D 041702SCAN.M Thu Apr 18 09:37:41 2002 Page 6

NYC-WTC_000047935