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GCMS analysis results for sample AE08426, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048169–000048181

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048177
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08426.D Vial: 13 Acq On : 19 Apr 2002 7:57 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: l. 00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 3-Penten-2-ol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 5.80 0.50 ug/1 688522 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-ol 86 C5H10O 001569-50-2 59 2 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 53 3 1-Hexene, 4,5-dimethyl- 112 C8H16 016106-59-5 50 4 Furan, tetrahydro-2-(methoxymeth... 116 C6H12O2 019354-27-9 47 Abundance Scan 463 (5.799 min): 08426. D (-457) (-) m/z 41.10 100.00% 41 71

5000

47 53 58 84

n/z-> 5 i" " I" ‘' i" " i" " r •" i — +7++ "'1'1' Lipo HHH 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 1 r'" r ■" i' 5.40 m/ z 5.60 71.10 5.80 6.00 97.48% 6.20

Abundance #24376:3-Penten-2-ol 43 71

............................................. ............ 5000 27 53 5.40 5.60 5.80 6.00 6.20 m/z 43.05 89.90% 58 86 HMil l|,...11 ■ 11 4 -mm 15

n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #24354:1,6-Heptadien-4-ol 43 71

5.40 5.60 5.80 6.00 6.20 5000 m/z 69.20 51.21%

27

| I I n | I ll l i?2 38 ., ,tll| 53 ■ ■ 11,1' | ■ > ■ ■ । EE■ 111111 , 79 84 94 1'”' i"" i ..................................... I" "I ’ m/z- > !5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #6302:1 -Hexene, 4,5-dimethyl- MA,A,A.A, N .A, 1 ’ I ' ' ' ' i ' ' 43 5.40 5.60 5.80 6.00 6.20 71 m/ z 39.10 48.07%

5000 55

27 15 , 77 84 97 i" " i ■ .... Ill...... |ll .... ................. ’ । > 111" I ■ >1111 ■" ।।1 < ■ < । < < >r । ■ -4A-4A— ---44 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 5.40 5.60 5.80 6.00 6.20

08426.D SCAN020418.M Thu May 02 15:30:23 2002 Page 5

NYC-WTC_000048177

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NYC-WTC_000048177Source: NYC Law Department, mirrored locally

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