GCMS analysis results for sample AE08427, May 2002

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Data File : C:\MSDCHEM\l\DATA\020419\08427 .D Vial: 14 Acq On : 19 Apr 2002 8:56 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 1-Hexene, 4,5-dimethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

5.80 0.34 ug/1 479810 1,4-Dichlorobenzene-d4 11.38 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 4,5-dimethyl- 112 C8H16 016106-59-5 36 2 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 32 3 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 23 4 Propanoic acid, 2-methyl-, anhyd... 158 C8H14O3 000097-72-3 23 Abundance Scan 464 (5.805 min): 08427.D (-458) (-) m/ z 41.10 100.00% 41 71

5000

53 RO 84 5.40 5.60 WA 5.80 6.00 6.20

n/z-> . .... 36 48 58 1111 /1 j 111 ■ । ■ 111111 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 m/ z 43.10 86.25% Abundance #6302:1 -Hexene, 4,5-dimethyl- 43 71

5000 55 —YYY------ 5.40 5.60 5.80 6.00 6.20 27 m/z 71.10 81.47% 15 - TTT-rpT-rq-rrrfp- 65 +5Q— H .• ■<।77 84 97 <1•11>■»11>! 111... ■ 11,,! ।,1 ■> ।, nz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #109335:1,6-Heptadien-4-ol 4(3

71 —HT 5.40 5.60 J, । A 5.80 6.00 6.20 5000 m/ z 69.10 51.19% 27

15 ... I" " I' 1 . THTTH38 , 53 65 ,, '1' ।" 79 1TTNTTTT 97 ■11' ■ ■ ■ i ■ ■1 ■ i"' ■ i ■ ■ ■11 ■ ■" i' mfe-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #24354:1,6-Heptadien-4-ol 43 71 .. y , , /u 5.40 5.60 5.80 6.00 6.20 m/z 39.20 50.95% 5000

27

n/z—> 1+11,32.3f 1" ' i" " i'1" i' 53 TTHTTH 65 I +73,84 94 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 I >"11 ■11 > I > >" I < 45.40 5.60 5.80 6.00 6.20

08427.D SCAN020418.M Thu May 02 15:34:21 2002 Page 4

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