GCMS analysis results for sample AE08426, May 2002

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Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048169–000048181

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08426.D Vial: 13 Acq On : 19 Apr 2002 7 : 57 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.27 ug/1 592393 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 80 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 72 3 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 59 4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 50 Abundance Scan 4768 (31.094 min): 08426.D (-4760) (-) m/z 192.05 100.00% 192

5000 40

51 70 82 9 112 146 160 —— 30.80 31.00 31.20 31.40 111"11 ■1 TT‘ TT 1 I " " h‘ । ■ । . ll . ,, n i |i i, 111 11 i 11 i i i । । I'l i । । i i i'| i i I’ m/z 40.10 36.22% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125847: Anthracene, 2-methyl- 192

5000 30.80 31.00 31.20 31.40 m/ Z 191.00 26.31% 28 39 51 63 82 96 115 126 139 152 165 I , l /O ' r 1 ■ ' i ■11 ''I' ■' ■ I'1' ■' i'''1 ■ r ri ■ t1' rt 11 *Imuu“mntnI t'l t I I tr mt ‘111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

30.80 31.00 31.20 31.40 5000 m/z 146.05 11.32%

m/z-> 29 39 51 63 74 83 I . 96 115 126 139 152 ‘I‘***IIdI‘I‘nnvprud‘t"ooo/edhn I 1 ' 11 Thu ITT I | I PI I | I I I I ] > Ir I ! I I |'I ! I I | 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 165 176 TTTHT 4— Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- ' 1 I ’ r ’ ’ I > » ■ i ■ ' ' ■ i ■ ■ 192 30.80 31.00 31.20 31.40 164 m/z 193.00 10.99% 5000 99 115 47 77 177 67 125,34 146 m/z-> 27 TT—THr 381457, +87—+ll4,+1155. p4 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

08426 .D SCAN020418.M Thu May 02 15:30:24 2002 Page 6

NYC-WTC_000048178

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GCMS analysis results for sample AE08428, May 2002 · Box DEP Box 27

NYC-WTC_000048195

Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.

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