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GCMS analysis results for sample AE07975, April 18, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07975 conducted on April 18, 2002.

NYC-WTC_000047577–000047592

Folder label: “GCMS X 4/4/02 A 4/15/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020415\07975.D Vial: 15 Acq On : 15 Apr 2002 10:15 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene, 2-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 22.64 0.23 ug/L 303705 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 2/Phenanthrene, 9-methyl­ 192 C15H12 000883-20-5 53 ’S Anthracene, 2-methyl- 192 C15H12 000613-12-7 50 4 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 45 Abundance Scan 3330 (22.645 min): 07975.D (-3319) (-) m/z 192.30 100.00% 192

5000

—PPP P9 96 146 160 n/z—> 01 ■ i 40 52 66 i"" 111 uj 11 ----- . 118 ................. 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 2240 22.60 22.80 23 00 m/z 191.30 24.48% Abundance #125847' Anthracene, 2-methyl- 192

5000 2240 22.60 22.80 23.00 m/z 193^30 17.00% 96 165 28 39 51 63 74 82 . 115 126 139 152 । 176184 I I 01 ■ । ■ > ■ I 11 1 1 1 "| i i i I | । । । । । Pc1 1 | ' f‘ri j‘1*i pf| i । । i’[ tti r| ri 11 । > i । i‘| 11 rrthrr i| 111 i rl 11 । । | *| | ri i [ < > n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

22.40 22.60 22 80 23 00 5000 m/z 146.30 14.73%

n 29 39 51 63 75 83 25 115 126 139 152 165 176 I | U ' I " " I ■ " ' I " " I1 " ' I' I "*1 r11 "fI | I'l | 11 I I I | I ri l | I I I I |, I > I i r, I'l 1, 11 t’t i |, ch |, , dt’I’t “ I" n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125845 Anthracene, 2-methyl- .............A............. , 192 2240 22.60 22.80 23.00 m/z 96.20 11.62%

5000

96 165 67 75 88 । 115 126 139 152 | ,1^6 0 *T*PPphmT 4rspi‘.... ...... . Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22 40 22.60 22.80 23 00

07975.D 041202SCAN.M Tue 'Apr 16 13:45:22 2002 Page 10

NYC-WTC_000047590

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NYC-WTC_000047590Source: NYC Law Department, mirrored locally

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