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GCMS results sample AE08255, April 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08255 showing surrogate recovery and unknown compounds from April 2002.

NYC-WTC_000047867–000047885

Folder label: “GCMS X 4/8/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08255.D Vial: 13 Acq On : 17 Apr 2002 7:22 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 10 Anthracene-d10- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

23.18 0.53 ug/L 826983 Phenanthranene-dlO 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 90 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 4 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 40 Abundance Scan 3420 (23 174 min) 08255.D (-3412) (-) m/z 188.10 100.00% 188

5000 ........ / 80 94 U’ ’ ' I 54 6641 112 132 146 160 22 80 23 00 23 20 23.40 23.60

n/Z— > 0-7 H TTHTHTHm TTT7H+ tmn 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 189.10 20.36% Abundance #79826 Anthracene-d10- 188

5000 ‘ I 1 1 1 1 1 22 80 23.00 23 20 23.40 23.60 m/z 94.05 15.33% 80 94 160 i 66 17 3 0 42 52 118 132 146 .|| 170 1801. 1 ,| 102 0 TTT ''i11'1111111111111111 —HH — TPNTTtTTT I" " I /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ........... / TIT 22 80 23 00 23 20 23.40 23.60 5000 m/z 184.05 15.06%

80 94 160 30 42 52 66 -n/Z-> 0 TWPTtH —02110118. .132.146, 170.180—— 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 T

Abundance #79739: Cycloheptanone, 4-phenyl- ' i 1 ■ ■ 1 i i r ' 1 ■ i ■ 188 22.80 23 00 23 20 23 40 23.60 117 104 m/z80.10 13.34% 91 160 5000 131 170 27 39 51 65 78 145 0 -j-.-r,, [ i i J.'t i i nV#, i-. lulppsileadpoal ++, Hl TITT It '1 "111 frrn ............... .............. n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23 20 23 40 23.60

08255.D 041702SCAN.M Thu Apr 18 09:25:00 2002 Page 14

NYC-WTC_000047884

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NYC-WTC_000047884Source: NYC Law Department, mirrored locally

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