GCMS analysis results for sample AE07976, April 18, 2002

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Laboratory report documenting GCMS analysis of sample AE07976 conducted on April 18, 2002.

NYC-WTC_000047593–000047607

Folder label: “GCMS X 4/4/02 A 4/15/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020415\07976.D Vial: 16 Acq On 15 Apr 2002 11 : 05 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 7 Anthracene-d10- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 23.17 0.44 ug/L 538303 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene - dl 0 - 188 C14D10 001719-06-8 91 2)Phenanthrene-dlO 188 C14D10 001517-22-2 78 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 42 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 Abundance Scan 3420 (23.174 min) 07976.D (-3414) (-) m/z 188.40 100.00% 188

5000

/ t 40 22.80 23 00 23 20 23.40 23 60 01' |" " l" ' 'I'' 66 80 .J 132 158 180 "I"" plliyem l(ll U ('ill I | l I. I J | 111 jn M | |, | L| I l ( > rPeero I | " I I | 1 m/ z 189.40 15.75% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826 Anthracene-d 10- 188

5000 22 80 23.00 23.20 23 40 23.60 m/z 94.30 15.10% 80 94 160 17 30 42 52 66 | | 102 118 132 146 || 170 180 0-T ■ ■11 ■ ■ ’11 ■ । ■ 11 ■ ■ ■ 111 > । . ....... . I"-'111" I 7'' i'I' ■ ■' 111 ■ TTT t-TTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827 Phenanthrene-d10 188

22 80 23 00 23 20 23.40 23.60 5000 m/ z 80.30 11.97%

80 94 160 30 42 52 66

ti/z—> l| 102110118 132 146 0 1111'' 111 rl l rmttrri 1111111111 prh " 111 11'111 ■ ■ ■ |1 ■ " | "1111 r ■ 11 ■ l ■ | ■ r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 170.189 —— Abundance #79804. Naphthalene. 1.7-dimethoxy- TTT ' I ' 173 188 22 80 23.00 23.20 23 40 23.60 m/z 184.30 11.06% 5000 102 115 145

51 63 75 94 130 158

n/z-> ov m11''' I ml... 10 TPTPTTT p 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 80 23 00 23.20 23.40 23.60

07976.D 041202SCAN.M Tue Apr 16 13:46:09 2002 Page 10

NYC-WTC_000047606

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GCMS analysis results for sample AE07977, April 18, 2002 · Box DEP Box 27

NYC-WTC_000047608

Laboratory report documenting GCMS analysis of sample AE07977 conducted on April 18, 2002.

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