GCMS results sample AE08258, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08258.D Vial: 16 Acq On 17 Apr 2002 9:50 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C: \MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 14 Anthracene-dlO- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

23.17 0.56 ug/L 905950 Phenanthranene-dlO 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 90 2 Phenanthrene-dlO 188 C14D10 001517-22-2 80 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 53 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 Abundance Scan 3420 (23 174 min). 08258 D (-3414) (-) m/z 188.10 100.00% 11 8

5000

80 94 22 80 23 00 23.20 23 40 23.60

/z-> 0-mmmp —| 43 49 49 57 66 WU 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z94.10 15.81% Abundance #79826 Anthracene-d10- 188

- 5000- 22 80 23 00 23 20 23 40 23 60 80 94 m/z 189.10 14.36% 160 , । 52 66 m/z-> 17 30 42 0- i1"11"1 ■i" " i1 ■ .......... Ij + TITTWTTTTTT 102 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TT 118 132 146 4.170,1894— Abundance #79827 Phenanthrene-d10 188

22.80 23 00 23 20 23.40 23 60 5000 m/z 184.10 13.04%

80 94 160 30 42 52 66 1 102110118 132 146 .1 0^........ I ‘1'11' ■1 ■ I" '' I H 111'1111■ ■ I'! I''' 'I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771: 3-Amino-4-methy-6-methoxyquinoline 188 1 — m. 22 80 23 00 23.20 23.40 23.60 m/z 80.00 12.29% 145 5000

117 159 173 41 51 63 77 89 102 130

/z--> 0-7 । I . rlir i rille, । 4 lr . i r|l. । ,|'l'i ।. 111 il ।, n ,.. 111ill, । i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 > rrl I I | JU 7 ‘d I ’ ■ ■ 1 1 ■ 22 80 23 00 23 20 23 40 23 60

08258.D 041702SCAN.M Thu Apr 18 09:37:44 2002 Page 19

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