GCMS results sample AE08258, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08258.D Vial: 16 Acq On 17 Apr 2002 9:50 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 Diftalone Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

35.03 0.20 ug/L 220369 Perylene-dl2 34.79

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Diftalone 264 C16H12N2O2 021626-89-1 9 2 Dispiro[4.1.4.1]dodecane-6,6,12,... 264 C16H16N4 074764-30-0 9 3 N-Acetyltranylcypromine 175 C11H13NO 078682-61-8 7 4 Benzofuran, 7-methyl- 132 C9H80 017059-52-8 5 Abundance Scan 5437 (35.025 min): 08258.D (-5435) (-) ”m/z 40.00 100.00% 4)

132 5000 262 116 34 60 34 80 35.00 35 20 35.40 208 0-P 1 I ' • ■ 1 i 1 1 ■ ' i ' 1 1 r ■ ■ > ■ I ■ ■ । । । । ■ ■ ■ i ■ ■ ■ ■ । ' 1 1 1 । । 1 ' 1 । m/z 132.20 53.75% /Z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 #122112: Diftalone 13 2

264 5000 90 34.60 34.80 35.00 35.20 35.40 105 118 m/z 131.50 49.25% 51 63 7 0)* ।111 1 ।111ll l’ I r1L 1 Alaik I ill ill I. 1______________________ 235 r" 11 nrr i-i"l ‘ 1 r ' I ■ ' 1 ' I ' ' 1 I ' ' 1 1 1 1 ‘ ‘ ' I ' -PPP .

Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #59759 Dispiro[4.1.4.1]dodecane-6,6,12,12-tetracarbonitrile 112

34 60 34.80 35 00 35 20 35.40 5000 264 m/z 2 62.10 38.00% 41 67 196 235 27 I w 53 iJ 78 91 104115 145 155 170 . 208 222 _ n/z-> 0 20 I 4, 440 Vl^ 1440p,4lt-/14e-pr"lhr 4* .-V1!1. 60 80 100 120 143155 182 1-1-1 pdhpi-dteialph, rhe mdei r 140 160 180 200 220 1242. 240 260 Abundance #59666: N-Acetyltranylcypromine 13 2 34.60 34 80 35.00 35 20 35.40

116 m/z 129.70 32.75% 5000 60 84

105

n/z-> Oli............11 1 20 40 60 80 LLL 100 120 140 146157 160 175 180 200 220 240 260 34 60 34.80 35 00 35.20 35.40

08258.D 041702SCAN.M Thu Apr 18 09:37:45 2002 Page 20

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