GCMS blank results for VOCs, sample AE12326, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\LBA.D Vial: 14 Acq On : 29 May 2002 8:41 pm Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Diftalone Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 34.90 0.20 ug/L 76076 Perylene-dl2 34.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Diftalone 264 C16H12N2O2 021626-89-1 37 2 Dispiro[4.1.4.1]dodecane-6,6,12,... 264 C16H16N4 074764-30-0 9 3 Cycloocta [1,2-b:4,3-bz :5,6-b" :8. . . 264 C16H804 056598-42-6 7 4 5H-Dibenzo[c,f][1,2]diazepine, 3... 264 C13H10C12N2 000955-66-8 7 Abundance Scan 5416 (34,901 min): LBA.D (-5414) (-) m/z 131.90 100.00% 132 264

5000 281 40 208 34.60 34.80 35.00 35.20 0: I’t * i1 ■ • ■ i ■ ■ ■ ■ i ■ ■ • ‘ i • ■ ■ i ' ■ ■ • i ■ ■ ■ • i m/z 264.10 82.03% n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #122112: Diftalone 132 264 5000 90 - ■ 11 > > ■ >-r> ’11 34.60 34.80 35.00 35.20 105118 m/z 132.90 77.78% , 51 63 1177 235 niz-> 0 -ll ilk th I Il... 1_ . .......... TI 1 ‘ ‘ 1 ! ’ * * ‘144 ‘ * • I ‘ ‘ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 . .......... .......... ’ I * ' * ‘ I ‘ ‘ ‘ I ' ‘ 'L ‘ ’ ' I 11 • • । ■ ■

Abundance #59759: Dispiro[4.1.4.1 dodecane-6,6,12,12-tetracarbonitrile 132 l 34.60 34.80 35.00 35.20 181

5000 264 m/ z 132.30 68.30% 41 67 196 235

iz-> 0 20 7> i 53 55 79 91 104,. 4, - APm, |-W I ll mr ah ,>| 40 60 155 170182 | 208 222" 249 —mrfprhrh1 r" il । r‘ 1"a 11 80 100 120 140 160 180 200 220 240 260 280 * > i • •

Abundance #95118: Cycloocta[1,2-b:4,3-b':5,6-b“:8,7-b",]tetrafuran - TTBT—n/n/i 264 34.60 34.80 35.00 35.20 234 m/z 259.00 52.94% 152 5000 132 208 75 179 43 63 i ................... 0 i ■ ‘ ■ ■ i ■ ■ ■ ■ i' ■ I • ‘ ‘ ‘ I ’ • ’ ‘ I ’ ' 1' i ■ l....... .......... ■ ‘ i ■ ■ ■ ■ i ■ * •' i ■ ■ i' ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

LBA.D 052202. M Mon Jun 03 11:28:20 2002 Page 19

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