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GCMS analysis results for sample AE00840, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.

NYC-WTC_000052108–000052127

Folder label: “GCMS X 1/11/02 A 1/31/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02JAN31\00840.D Vial: 4 Acq On : 31 Jan 2002 5:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise 2002 : January 31, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 4-(Dimethylamino)-1,3-diaza... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

9.65 0.08 ug/L 39187 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-(Dimethylamino)-1,3-diazaspiro... 209 C11H19N3O 000000-00-0 39 2 2-Propanol, 1,1'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 39 3 2-Propanol, 1,1'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 9 4 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 9 Abundance Scan 550 (9.653 min): 00840. D (-) m/z 59.10 100.00% 59

5000

0-T । ■1" r 45

i 73

r "' i" " i 86 103

i" " r "' r ■" i i ■'" i" " i m/ z 9.40 A 45.10 9.60 9.80 1112 10.00 45.17% m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #128682: 4-(Dimethylamino)-1,3-diazaspiro[4,6]undec-3-en-2-on 59

45 5000 1 • l । ■ ■ 1 i 1 ' ■ ■ i ' 1 ' • i ■ ■ 9.40 9.60 9.80 10.00 73 m/z 41.10 30.26% 103 209 01 ■i11111 i" " i ■" ■ i" " i " " r "' i" " i" " i ’"11" " i" " i" " i" " i" " i TVTTTTTTTTT n/z-> 20 : 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundances #29204:2-Propanol, 1,1 '-oxybis- (CAS) $$ Dipropylene glyc... 59 • ■ i ■ 1 1 ' i TT—dm 9.40 9.60 9.80 10.00 31 m/z103.10 27.95% 5000 45 103

n/z-> o1 4 Jt"111" " r" " i" " i'1" i" " i" " i" " i" " I'1" 11'" i" " i " " i"1' r "11" " i :20 30 40 50 60 70 80 90 100110120 130140150160 170180 190200210 Abundance! #29205: 2-Propanol, 1,1 ‘-oxybis- (CAS) $$ Dipropylene glyc... TTr’i T IL 59 9.40 9.60 9,80 ______________ 10,00 m/z 73.10 22.08% 31 5000 45 103

0 ।.,′′′ ... 1’’ n111।।।.11 I"111"111" " i" " i"" i" " r " ’ i"11 r'" i11" I ..... A/, /z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 9.40 9.60 9.80 10.00

90840.D SCAN508.M Fri Feb 01 09:19:21 2002 Page 9

NYC-WTC_000052120

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NYC-WTC_000052120Source: NYC Law Department, mirrored locally

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