Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
NYC-WTC_000037700–000037719Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report • Data File : C:\MSDCHEM\1\5973N\02MAR08\03611.D Vial: 1 Acq On : 8 Mar 2002 3:35 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 4-(Dimethylamino)-1,3-diaza... Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
9.58 0.09 ug/L 41886 1,4-Dichlorobenzene-d4 9.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-(Dimethylamino) -1,3-diazaspiro... 209 C11H19N3O 000000-00-0 3 2 ETHYL 4,4-D2-N-HEXYL ETHER 132 C8H16D20 005756-44-5 25 3 Butanamide, 3-methyl- (CAS) $$ 1... 101 C5H11NO 000541-46-8 25 41-Propanol,3-ethoxy-$$Dowanol...104C5H1202 000111-35-3 9 Abundance Scan 550 (9.583 min): 03511 .D (-) m/ z 59.00 100.00% 59
5000
0! 45
— 73 86 103
T 9.20 9.40 m/z 103.00 KN 9.60 9.80 47.30% 10.00
miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #128682: 4-(Dimethylamino)-1 ,3-diazaspiro[4,6]undec-3-en-2-on 59 45 5000 ■ i • 1 ■ • i • ‘ • 1 i
73 9.20 9.40 9.60 9.80 10.00 m/ z 45.10 44.12% 103 & | 209 Of 1 I 1 1 1 T ■ i ■ ■ >• r ■ 1 1 • i ■ • ■ 1 i ■ • • ■ i ■ ■ • ■ i ■• • • i ■ • • • t • •• • i miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #26982: ETHYL 4,4-D2-N-HEXYL ETHER 31 59 ■ i ■ ' ' ■ I ■ ■ 9.20 9.40 9.60 9.80 10.00 5000 m/ z 43.00 32.32%
N 47 86
Oi — 11 ■ — ■ I1 ! 1 Lt ' ■ i ■ ■ ■ ■ i • ■ ‘ ‘ i 1 ■ 1 1 i • ‘ ■ ■ i • ' ' ' i • • ‘ ■ i ' ‘ ‘ ‘ i miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #8825: Butanamide, 3-methyl- (CAS) $$ Isovaleramide $$ Iso... III • 59 9.20 9.40 9.60 9.80 10.00 m/z 44.00 24.34%
5000 44 29 86
miz—> 0 15 l , • • i • ■ • • i 20 40 69 --- 60 | 100 ......... — 80 100 120 • • i • • 1 • i ■ • • • । • • ■ ■ । • ■ • • । 140 160 180 200 9.20 9.40 Tr 9.60 IILL ’d" 9.80 10.00
03511.D HP022102.M Fri Mar 15 10:09:11 2002 Page 12
NYC-WTC_000037715
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NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006105
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03246 conducted on March 15, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.997
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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