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GCMS blank results for sample AE03611, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.

NYC-WTC_000037700–000037719

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037716
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03611.D Vial: 1 Acq On : 8 Mar 2002 3:35 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 3-Hexanol (CAS) $$ Hexan-3-... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

9.86 0.09 ug/L 43528 1,4-Di chlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H14O 000623-37-0 43 2 3-Hexanol 102 C6H14O 000623-37-043 3 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H14O 000623-37-0 43 4 3-Pentanol (CAS) $$ Diethyl carb... 88 C5H120 000584-02-1 40 Abundance Scan 575 (9.865 min): 03511.0 (-) m/ z 59.00 100.00% 59

5000

43 84 _M.L 9.60 TIPPY 9.80 10.00 10.20 O -HHl ,। . . .1! .... ।.... ।.... ।... 11... 1|. m/z 43.10 12.49% miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #9604:3-Hexanol (CAS) $$ Hexan-3-ol $$ C2H5CH(OH)C3H7 $$ ... 59

5000 73 9.60 9.80 10.00 10.20 AAA I 1 ' ‘ 1

m/z 73.00 12.24% 42 84 102 01 TpmRTTTHTTT +4 — +t T i*‘“i 1’101 miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #9599: 3-Hexanol 59 TIT T 9.60 9.80 P1 10.00 10.20 31 5000 m/z 41.10 10.41% 43 73

A 102 01 “ r “ ■ 11 ’ 1 mHHmpm 4 - p ।.... ।. i. ।.... । p 1 “ I I’ miz-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 #9602: 3-Hexanol (CAS) $$ Hexan-3-ol $$ C2H5CH(OH)C3H7 $$... 59 .. ALL 9.60 9.80 10.00 10.20 m/ z ■42.10 9.22% 31 73 5000

42 84 102 0 1111 “ ‘ 11 ’II mmmmm +4 Tp V TT i' ■" i TIpiy -A4 -- m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 9.60 9.80 10.00 10.20

03511.D HP022102.M Fri Mar 15 10:09:12 2002 Page 13

NYC-WTC_000037716

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NYC-WTC_000037716Source: NYC Law Department, mirrored locally

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