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GCMS results for sample AE00469, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00469 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051471–000051484

Folder label: “GCMS X 1/8/02 A 1/11/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00469.D Vial: 8 Acq On : 11 Jan 2002 7:55 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Hexanol Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 9.85 0.10 ug/L 38946 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 9 2 1,2-Butanediol (CAS) $$ 1,2-Buty... 90 C4H10O2 000584-03-2 9 3 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H14O 000623-37-0 9 4 Butane, 1-ethoxy- (CAS) $$ Ethyl... 102 C6H14O 000628-81-9 9 Abundance Scan 567 (9.847 min): 00469.D (-) m/z 59.10 100.00% 59

5000

43 73 . A. ----------------------- 9.60 9.80 10.00 10.20

m/z-> 0+ —9 । 84 i11 " r ■ " I ■' I' I' ■ " i " '11" " r " ' i" " r ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/z 43.10 11.75% Abundance #9599:3-Hexanol N 59 J

31 5000 43 73 9.60 9.80 10.00 10.20 m/z 45.00 11.67% 102 m/z-> 0 1 ■ r " 11' TTT —l. . 4 T 11’00001-000—— 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #5245:1,2-Butanediol (CAS) $$ 1,2-Butylene glycol $$ .alp... 59

9.60 9.80 10.00 10.20 5000 43 m/z 41.10 10.58%

88 A 0 111" " i " " i " " i " — i" " r " 11" " i111' i " 1' i'1" i " " i " " i1 m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #9600: 3-Hexanol (CAS) $$ Hexan-3-ol $$ C2H5CH(OH)C3H7 $$ ... 59 A9.60 9.80 10.00 10.20 ■ ■ i ' ‘ ■ i ' ’ ■

m/ z 58.00 8.72% 31 5000 73

44 m/z-> 0 ‘' i " " i' rrf + ... I'll... 1.... । 102 ■ r ■ " r "' i " " i " '' i" " I'1" i1' " i1 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ' 1 1 1 ' ' ‘ i 9.60 T-r-p-r-r-r-p-r 9.80 10.00 10.20

00469.D SCAN508 .M Mon Jan 14 10:47:11 2002 Page 7

NYC-WTC_000051481

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NYC-WTC_000051481Source: NYC Law Department, mirrored locally

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