GCMS analysis report for sample AE01507, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01508.D Vial: 8 Acq On : 21 Feb 2002 9:01 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 3-Hexanone (CAS) $$ Hexan-3... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T.

4.81 0.06 ug/L 28922 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone (CAS) $$ Hexan-3-one ... 100 C6H120 000589-38-8 72 2 3-Hexanone (CAS) $$ Hexan-3-one ... 100 C6H120 000589-38-8 72 3 3-Hexanone (CAS) $$ Hexan-3-one ... 100 C6H120 000589-38-8 50 4 3-Hexanone (CAS) $$ Hexan-3-one ... 100 C6H120 000589-38-8 50 Abundance Scan 127 (4.808 min): 01508.D (-) m/z 43.10 100.00% 43 57

5000 71 100 AA MA., 1114 51 4.40 4.60 4.80 5.00 5.20 0 ■■i■■■■i■■ “ i ■' ■ ■ i “ • ■ i I’ ''11 ■'111 ■ ■ i ■• ••i■ ■ • ■ i ■ ■ i • • 84 i “ ■' i" i •' ■ ■ i' ‘ ■ ■ ■ i •' ‘' i m/z 57.00 89.80% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #8262:3-Hexanone (CAS) $$ Hexan-3-one $$ Ethyl propyl ket... 43 57 71 5000 100 4.40 4.60 4.80 5.00 5.20 m/z 71.00 48.71% 85 0 —mp thpmmmmmp P miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #8263:3-Hexanone (CAS) $$ Hexan-3-one $$ Ethyl propyl ket... 43 57 i • ■ ■ ■ i ■ ' 1 1 1 ■ 1 I ■ 1 71 4.40 4.60 4.80 5.00 5.20 5000 m/z 100.10 31.60% 100

Of TTTTTTTTTTTH +ppt HW ITI—sduyuudatenvyraazyeuan * ,...... 85....... niz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #8256:3-Hexanone (CAS) $$ Hexan-3-one $$ Ethyl propyl ket... 43 4.40 4.60 4.80 5.00 5.20 57 m/z 41.10 27.70% 23 5000 71 100

/z—> t 0 •. i >1 • ■ i • tpr 85 —mmmmmmppm W—aa 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 4.40 4.60 4.80 5.00 5.20

01508.D HP022102.M Mon Feb 25 10:54:56 2002 Page 5

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