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GCMS results for sample AE00469, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00469 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051471–000051484

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051482
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00469.D Vial: 8 Acq On : 11 Jan 2002 7:55 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 6 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 78092 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 59 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 00469.D (-) m/z 192.10 100.00% 192

5000

96 40 0 TTt 66 82 . ..............................M 146 160 118 II 11' ■ ■ ■ i' ■ ■11 ■ ■ ■ • i'' 22.00 22.20 22.40 22.60 m/z 146.10 15.49% T‘[T /z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 ■nr A i ■ ■' 22.00 22.20 22.40 22.60 146 175 m/z 191.10 14.49%

Of T’—’EIUIIIr T’OIITTu’r 11 " " I" '> i' i ■ ■' ■ I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-cartx>nitrile (CAS 192

22.00 22.20 22.40 22.60 5000 m/z 193.10 14.29%

96 164 138 Of I''1■i■11'1" 1111111111" I " mmmTTPTT TTTT n/z- > 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene I" 1 1 11 I ' 192 22.00 22.20 22.40 22.60 m/z96.10 14.00%

5000

96 -|65 88al O- ।11111 ■ i1" ■ i11" r11111111 139 152 .1 V6 ,i TTunnm 111111" " r "11"111111 ri1"1111 "I' i "11 rTrr /z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

00469.D SCAN508.M Mon Jan 14 10:47:12 2002 Page 8

NYC-WTC_000051482

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NYC-WTC_000051482Source: NYC Law Department, mirrored locally

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