Gas chromatography-mass spectrometry analysis of sample AE00327 showing unknown compounds and surrogate 2,4-DDD measurement.
NYC-WTC_000051192–000051205Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02JAN10\00472.D Vial: 7 Acq On 10 Jan 2002 7:46 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 8 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 86530 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 53 4 1-amino-2-methyl -4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 00472. D (-) m/z 192.10 100.00% 192 I 5000
96 146 160 .. A.. * 22.00 22.20 22.40 22.60 70 82 44 0 ■ ■ i ■1' ■ r ■ ■ ■ i1 H - 118 v LL I m/z 96.00 15.81% m/z-> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 1 192
108 5000 22 00 22.20 22.40 22.60 146 175 m/z 193.10 15.54%
o >. 11' ।। . ■ > i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ • > i • > i ■ ■' ■ i " ■11' " 1111 r i' ■'' i'1'' i1 +TT 1111 m/z--> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 ................ 0 22.00 22.20 22.40 22.60 5000 m/z 191.10 14.93%
96 164 - 138 0 ------- 11 " 11111" i ■’T" n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 192 22.00 22.20 22.40 22.60 m/ z 146.10 13.73%
5000
91 165 119 147 131 - 103 I___ IL I 177 A 0-TTT I T’T’TTTTIITIITuI — + i 1 ■ 1 'i m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
00472.D SCAN508.M Fri Jan 11 10:08:56 2002 Page 10
NYC-WTC_000051203
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000051088
Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051055
Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051422
Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051105
Laboratory report showing GCMS analysis of sample AE00318 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051301
Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051408
Laboratory report showing GCMS analysis of sample AE00462 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050793
Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049929
Laboratory report showing GCMS analysis of sample AD31637 including unknown compounds and surrogate recovery data.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051439
Laboratory report showing GCMS analysis of sample AE00464 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051073
Laboratory report showing GCMS analysis of sample AE00308 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049990
Laboratory report showing GCMS analysis of sample AD31644 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006045
Analytical report showing surrogate recovery data for sample AE03184 analyzed on March 15, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
Filed in the same folder
NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
Filed in the same folder
NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder