GCMS analysis results for sample AE00327, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis of sample AE00327 showing unknown compounds and surrogate 2,4-DDD measurement.

NYC-WTC_000051192–000051205

Folder label: “GCMS X 1/8/02 A 1/10/02”

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Data File : C:\MSDCHEM\1\5973N\02JAN10\00472.D vial: 7 ' Acq On 10 Jan 2002 7:46 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-Cyclohexene-l-carbonitril... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

9.94 0.13 ug/L 43523 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyclohexene-l-carbonitrile $$ ... 107 C7H9N 000100-45-8 83 2 cis-1,3-Cyclohexanedicarbonitril... 134 C8H10N2 010340-01-9 53 3 cis-1,3-Cyclohexanedicarbonitril... 134 C8H10N2 010340-01-9 53 4 Cyclobutane, 1,2-diethenyl- $$ C... 108 C8H12_ 002422-85-7 47 Abundance Scan 575 (9.938 min): 00472.D (-) m/z 54.10 100.00% 54

80 107 5000 39 67 92 ■ ' । । । ’ I > 1 A , . । i । । ' ■ i 1

m/z-> 0- 20 -l 30 40 5060 70 80 ..... Il . 90 100 110 120 130 140 9.60 m/z 107.10 9.80 10.00 10.20 52.45% Abundance #10985: 3-Cyclohexene-1 -carbonitrile $$ 3-Cyclohexenyl cya... 54

39 5000 । । • Tdr v 27 80 9.60 9.80 10.00 10.20 67 107 m/z 80.00 50.16% 92 O'l | 1 ! , .... II ■ i ■ ■ 1 ■ । r ■ ■ ■ ।1 ■ ■ i 1 ■ 1 1 i ■ ' , ■ ■ >1111 ■ ■ । । ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29419: cis-1,3-Cyclohexanedicarbonitrile $$ 1,3-Cyclohexa... 54 .A. 9.60 9.80 10.00 10.20 5000 81 m/ z 39.10 40.55% 41 67 107 94

134 m/z-> 01 .20— 30 ! A 40 50 60 1 ' i ' 1 1 1 i ' ' 70 1 I' ■ ‘ 1 1 ■ 80 90 ' 1 1 1 1 1 1 I ■ ■ ■ ' i ' ' ' ' i ' 1 ' ' i ' ' 100 110 120 130 140 Abundance #29418: cis-1,3-Cyclohexanedicarbonitrile $$ 1,3-Cyclohexa... ----- 54 9.60 9.80 10.00 10.20 m/z 41.10 38.78%

5000 81 41 67 107 94

134 0 ............ ..... II ' ' i ' ' 1 1 i 1 ' ■ ■ I ■ i'11 । । । । । ' I . । । > । ■ 1 । ’ 1 ■ ■ i ■ ■ ' i 11 11 1"" 1 1 i ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 9.60 9.80 10.00 10.20

00472.D SCAN508.M Fri Jan 11 10:08:56 2002 Page 9

NYC-WTC_000051202

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NYC-WTC_000051202Source: NYC Law Department, mirrored locally

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