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GCMS analysis results for sample AE00327, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis of sample AE00327 showing unknown compounds and surrogate 2,4-DDD measurement.

NYC-WTC_000051192–000051205

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051204
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00472.D Vial : 7 Acq On 10 Jan 2002 7:46 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.28 ug/L 168318 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Anthracene-dlO- 188 C14D10 001719-06-8 64 4 Acridine-D9 188 C13D9N 000000-00-0 50 Abundance Scan 1699 (22.771 min): 00472. D (-) m/z 188.10 100.00% 188

5000 94 80 49 66 160 | 22.40 22.60 22.80 23.00 23.20 , . 132 OT TTPHT 11 " 11 " । Io > ’ । . 111 |l m/ z 94.10 23.25% /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 TI a ■ ' i ' 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80-00 15.49%

m/z-> 0 i'11111'1' i ■ ■1 ■ 11 40 50 60 66 70 TTIt 80 i1''' i ■ ■'' i ■ ■ ■ ■ i' ■ ■ ■ i 90 100 110 120 130 140 150 160 170 180 190 158 i111H11111 —l— Abundance #84499: Phenanthrene-d10 188

22.40 22.60 22.80 2300 23.20 5000- m/z 189.10 15.34%

80 160 66 mlz-> O-PTIT 40 50 P 1r _Q I *''1 I 'rl 11 ■''' 111 r' 111111 1111 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 13.27%

5000

66 160 , .

m/z-> 0 । ■ ■ ■ ■ । ■ •1 ■ । ■ l ■ । ■ II..... 189... 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 i ■ ■ ■ ■ i ■ ■ ■ ■ । ■ ■ ■ • । ——————— 22.40 22.60 22.80 23.00 23.20

)0472.D SCAN508.M Fri Jan 11 10:08:56 2002 Page 11

NYC-WTC_000051204

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NYC-WTC_000051204Source: NYC Law Department, mirrored locally

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