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GCMS analysis results for sample AE00100, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050354–000050369

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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Scanned page image, NYC-WTC_000050367
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN23\00100.D Vial: 3 Acq On : 23 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN50 8. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.26 ug/L 158720 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 3 Acridine-D9 188 C13D9N 000000-00-0 56 4 anti-10-hydroxy-5,6,8,9-tetrahyd. .. 188 C12H1202 055139-53-2 50 Abundance Scan 1699 (22.771 min): 00100.D (-) m/z 188.10 100.00% 188

5000

80 - 1 ' i ■■ ■ ■i ■ 22.40 22.60 22.80 23.00 23.20

n/z—> 49 0 --- 64 > . ..... 132.. 160. .ill.. 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 189.10 14.52% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 1$8

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.05 13.26% 66 158 0 mPPTTTT TTTTt Pmmmmpmmmmmm niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 1118

2240 22.60 22.80 23.00 23.20 5000 m/z 94.10 12.17%

80 94 160

/z—> 66 0 I' " ■ 11 “ H 111111 > । 40 50 60 70 t

80 —1— । I i 111 I I ■ । I i i 11 i I I I | > 111 111 I । | i 11 r 11i 4 iiii .

90 100 110 120 130 140 150 160 170 180 190 , .

Abundance #85255: Acridine-D9 188 22.40 22.60 22.80 23.00 23.20 m/z 184 .10 8.28% 5000

93 158 66 80 — m/z—> O - 40 50 60 70 80 ' i ■1 ■ ■ i ■ ‘ ■11 ■ ■ ■ ■ i ■ ■ ■ ■ i1 ■ ■ • i ‘ ■ 90 1(X) 110 120 130 140 150 160 170 180 190 ll 22.40 22.60 22.80 23.00 23.20

00100.D SCAN508.M Thu Jan 24 09:57:10 2002 Page 10

NYC-WTC_000050367

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NYC-WTC_000050367Source: NYC Law Department, mirrored locally

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