GCMS analysis results for sample AE03075, March 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB28\02715.D Vial: 5 Acq On : 28 Feb 2002 1:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1 R.T. EstConc ■ Area Relative to ISTD R.T. 22.77 0.47 ug/L 333997 Phenanthrene-dl0 22.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 59 2 C14 H20 hydrocarbon 188 C14H20 000000-00-0 50 3 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 43 4 Acridine-D9 188 C13D9N 000000-00-0 42 Abundance Scan 1718 (22.768 min): 02715.D (-) m/z 188.10 100.00% uta

5000 94

49 132 80 160 22.40 22.60 22.80 23.00

mfe-> 0- +4 64 mpH* Tom TT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.00 28.46% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 108

5000 —TIIBTOTTTRTIT 22.40 22.60 22.80 23.00 80 94 m/z 189.10 22.18% 158 0- TIPPT 66 nuutt PmPPITmTP 11.... miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98620: C14 H20 hydrocarbon 118 --------- 22.40 22.60 22.80 23.00 5000 m/z80.10 12.60% 79 . 9 106 117 131 145 159 miz-> 0- * I ‘ ‘ ‘ ‘ I'' ‘ 40 50 60 ‘ ' I ‘ - 70 80 90 100 110 120 130 140 150 160 170 180 190 i “ “ i ‘ ■ IL Abundance #98584:2,2,9,9-Tetramethyldec-5-ene-3,7-diyne 188 22.40 22.60 22.80 23.00 ‘ ‘ ' 173 m/z 184.10 9.36% .. 131 143 5000 77 158 119

n/z—> 0- ‘11 ■ ■ ■ ■ i •1 ■ ■ i ■ “ ■ i ■ " ‘ i ■ ■ • • i ■ ■ “ i ■ ■ ■ ■ i ■ ■ 40 50 60 70 80 11’3 asipadasqaaipann 90 100 110 120 130 140 150 160 170 180 190 I “ ‘ ‘ I ------- 22.40 22.60 22.80 23.00

32715.D HP022102.M Fri Mar 01 10:07:08 2002 Page 14

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