GCMS analysis results for sample AE03075, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

NYC-WTC_000010907–000010926

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

: Data File : C:\MSDCHEM\l\5973N\02FEB28\02715 .D Vial: 5 Acq On : 28 Feb 2002 1:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Phenanthrene, 9-methyl- $$ ... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.12 ug/L 86952 Phenanthrene-dl0 22.64

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 1675 (22.282 min): 02715.D (-) m/z 192.00 100.00% 192

5000

82 96 146 ■ 1 i ■ ■ ■ ■ i ■ ■ 160 22.00 22.20 22.40 22.60

/z—> 0 44 PT 70 I 118 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 mll—p m/z 193.00 17.36% Abundance #103936: Phenanthrene, 9-methyI- $$ 9-Methylphenanthrene 19/2

5000 22.00 22.20 22.40 22.60 m/z 191.00 17.04% 96 165 88 ,,| 139 152 , | 176 , , 0 111 .1. . ।. 11 IPrmT 111' 111111. 111 . Pl. 11.. 111 r r. 11.।I... । .'I1. . (. . 1. j .. .’1 J1 Wpr miz—> 20 30 40 50 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 96.00 16.80%

54 110

iz—> 0- 30 “ i “ i ■ 1113117111171 94 -I'll.. r TTTTTTTTTTTTTTTTTTTTTHTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 160 U Abundance #102494: N-(2-methylprof>-2-enyl)-2-nitrobenzenarnine 192 22.00 22.20 22.40 22.60 77 151 m/z 146.10 16.45% 130 93 104 5000 119

177 0 1’1’111111112211119111711"’1""’’1 T-rp- TI’I I’T . .............. ’ I- 11’* .. । n ». ।». ।.!. ।. . । r* •1 iT 1. ......... A......... /.2. m/z—> 20 30 40 50 60 70 80 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02715.D HP022102.M Fri Mar 01 10:07:08 2002 Page 13

NYC-WTC_000010923

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GCMS analysis results, sample AE02718, March 2002 · Box DEP Box 14

NYC-WTC_000010967

Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.

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