DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\30704.D Vial: 1 Acq On : 1 Feb 2002 2:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 N-(2-methylprop-2-enyl)-2-n. .. Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 88442 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N- (2-methylprop-2-enyl) -2-nitrob. . . 192 C1OH12N202 000000-00-0 46 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 42 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 40 4 Pyrazine, tetraethyl- (CAS) $$ t... 192 C12H20N2 038325-19-8 40 Abundance Scan 1656 (22.280 min): 30704.D (-) m/z 192.10 100.00% 192

5000 96 146 160 m n/z—> 0 42 66 oM ‘ 1‘4‘‘111111‘‘141‘/-‘11‘411111*1**111818* 82 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l. 22.00 22.20 22.40 22.60 m/ Z 96.10 23.61% Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 77 151 130 93 104 5000 119 22.00 22.20 22.40 22.60 m/ Z 191.10 17.43% 177 0 ■ ■ । । ■ i ■ ■ ■11 ’ ■ ■' i1 ■ ■ ■ i ■ ■ "i ■ ■ ■ ■ । I’ TT‘ T’I’ .1 I ..... ""I111 ‘I1'11I 111'I 1. n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl-$$ 9-Methylphenanthrene 192

22.00 22.20 22.40 22.60 5000 m/Z 146.10 15.60%

96 w +U 165 0 ......................... 88.1, 139 152 ' i " " 11 r " i11 "'I ‘ ' i1" 176 TTTTTT m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline C 192 22.00 22.20 22.40 22.60 m/z 193.10 14.86%

5000 82

54 110

n/z—> 30 I 94 0 -H '1 r ' " i " 11111 '11111' I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TIIWTTITNTWWWTIWTTWTTTTTTT 160 U ...... H..... fl 22.00 22.20 22.40 22.60

30704.D SCAN508 .M Mon Feb 04 08:41:26 2002 Page 12

NYC-WTC_000004124

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999