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GCMS analysis results for sample AE00328, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00328 conducted on January 18, 2002.

NYC-WTC_000051206–000051221

Folder label: “GCMS X 1/8/02 A 1/10/02”

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Scanned page image, NYC-WTC_000051219
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00327.D Vial: 3 Acq On 10 Jan 2002 2:00 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 N-perdeuteriobenzylideneani ... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 76133 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 53 2 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 46 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H12O3 004497-40-9 45 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 Abundance Scan 1656 (22.280 min): 00327.D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.00 22.20 22.40 22.60 49 70 - 0 TTITTTIWTTTTTTTTTT i......... ’"I1 m/z 191.10 19.71% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 TT 22.00 22.20 22.40 22.60 54 110 m/z146.10 16.11% 30 I 94 0 mPPP " I " " I' mP 160 >»।" i " i" i" ■ ■ ■ i" i rl 4 TI j I > n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 77 151 / TTnTr । 1 ■ 130 22.00 22.20 22.40 22.60 93 104 m/z 193.10 14.96% 5000 119

177 0 mm r ‘ " i " " i " " I " "I •" ' i TT-ff nn/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 T’T TII’

Abundance #102611:2-Propenal, 3-(3,4-dimethoxyphenyl)- $$ Cinnamald... 192 22.00 22.20 22.40 22.60 161 m/z 96.00 12.77%

5000

77 149 177 64 89 193 118 138 0 . ...... I " i " " i" " i ■ ■" i'11' I" " I......... । >' 1111111111 ■ i" t /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

>0327.D SCAN508.M Fri Jan 11- 10:08:17 2002 Page 10

NYC-WTC_000051219

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NYC-WTC_000051219Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗

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