GCMS analysis results for sample AE03246, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03246 conducted on March 15, 2002.

NYC-WTC_000006105–000006125

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02MAR01\03246.D Vial: 1 Acq On : 1 Mar 2002 4:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 N-perdeuteriobenzylideneani ... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 103986 Phenanthrene -dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

I N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 46 3 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 000000-00-0 42 4 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 000000-00-0 38 Abundance Scan 1675 (22.283 min): 03246.D (-) m/z 192.00 100.00% 192

5000

96 146 160 1 ' 1 1 ' ' 1 1 I ' 1 ' 1 1 1 ' 70 82 22.00 22.20 22.40 22.60 42 । 118 + ।> 11111 > 11111111111"1' | 0 T" ' r| Il i i ! i ■ i ! j i 1 > > | I I l ■ | — m/Z 191.00 20.46% m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 22.00 22.20 22.40 22.60 54 110 m/ z 96.00 15.69%

n/z-> 30 0 '1111' " 11 ‘ ■111' '11" " i ■ > । ■ 1111 ■ > l94 ' H' ।' 11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 160 TTIUUTIWTTTTTTWWWTTTTITTTITT 1 Abundance #102494: N-(2-metbylprop-2-enyl)-2-nitrobenzenamine 19/2 77 151 , ....... ,1....... H 130 22.00 22.20 22.40 22.60 93 104 m/z 193.00 5000 14.76% 119

177 0 " ' i " '' i " " i " " i' ‘TTnutb' F’T "' 11 1111 ■" i ‘ 1.... ■ i ■ *" i" " i11" i" " i 111118 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102788:2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 22.00 22.20 22.40 22.60 164 m/z 146.10 13.26% A 5000 99 115 47 77 177 146 125 134 ......... A....... r 0 " i " ■' i" 111' ‘1 ■ i" 111" " I" " I " " 11111111" i1 -- lisas)) l..................... ‘11' " 11 " ■' I TII" mfz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

03246.D HP022102.M Mon Mar 04 12:33:14 2002 Page 13

NYC-WTC_000006121

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NYC-WTC_000006121Source: NYC Law Department, mirrored locally

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