Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
NYC-WTC_000050258–000050275Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN22\31664.D Vial: 1 Acq On : 22 Jan 2002 2:41 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 N-perdeuteriobenzylideneani ... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.13 ug/L 70386 Phenanthrene-dl0 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 2 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 58 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2: 000000-00-0 50 Abundance Scan 1656 (22.280 min): 31664.D (-) m/z 192.10 100.00% 192
5000 .............. ...... A
n/z—> .. ..... %. "J....... ........ I. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance Up 22.00 22.20 22.40 22.60 m/z 191.10 17.07% #88409: N-perdeuteriobenzylideneaniline 15 2
5000 82 T T 22.00 22.20 22.40 22.60 54 m/z 96.10 15.65% 110 30 94 160 Tnp < ■ i • • ■ ■ i ■' • • i - 1O9"Inpmmanp—mo2nonnt 1’111 /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624: 1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 192 -r-r-j-r-r-n-f T 22.00 22.20 22.40 22.60 5000 m/z 193.10 15.05%
................. 81 103 119 131 ..... . .... I TTTTpnnT7TTTTpTnTYrTTTpTT-rpn-rrYrrTTprrTTpTYrpnnT7TTTTpT^^ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192 22.00 22.20 22.40 22.60 m/z 146.10 12.11% 5000
144 177
iz—> .... I...H11I..j...»I.... 1.... J.... I. I.. 11... II. I >. 111. 20 30 40 50 60 70 80 90 1(» 110 120 130 140 150 160 170 180 190 200 L 1’111 ------- 22.00 22.20 22.40 22.60
31664.D SCAN508.M Thu Jan 24 14:00:07 2002 Page 10
NYC-WTC_000050271
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NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052069
Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051642
Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050317
Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050558
Laboratory report listing unknown compounds and surrogate recovery for sample AE00248 analyzed on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036779
GCMS analysis report for sample AD29522 listing unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011007
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02721 including surrogate recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010907
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
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NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
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NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
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NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
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NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
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