GCMS analysis results for sample AD31671, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.

NYC-WTC_000050024–000050038

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C : \MSDCHEM\1\5973N\02 JAN17\ 31671 .D Vial: 6 Acq On : 17 Jan 2002 6:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 1-amino-2-methyl-4-isopropy. .. Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 83048 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual l l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 2 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 46 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 45 4 2,4-Diamino-6~(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 42 Abundance Scan 1656 (22.280 min): 31671.D (-) m/z 192.10 100.00% 1912

5000

96 146 160 . ‘ ■ i ' ' ■ ■ i -P 82 22.00 22,20 22.40 22.60 44 70- 0 ■ ■ ■ i ■"' i'1 ■ TM —pp rn/z 191.10 17.06% /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192

5000 ' 1 1 1 1 1 ' I 1 1 ' 1 ' 22.00 22.20 22.40 22.60 144 177 m/z 96.00 16.30%

/z—> 0 T0a—nu2—n2—mmuumEgmmpm——mTu 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 rm Abundance #102494: N-(2-methyiprop-2-enyl)-2-nitrobenzenamine 192 77 151 130 22.00 22.20 2240 22.60 93 104 m/z 146.10 13.10% 5000 A 119 177 0 "'I‘ ’It l““ ••••|• > ['l > > > j l I I I J l > I1! PITn ‘rrrrn n/z—> 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline ................. / — *’)****I*’’I* 192 22.00 22.20 22.40 22.60 m/z 193.10 13.05% 5000 82

niz—> 30 0 Tm “ i ■ • "i‘ ■ mH 1 94 110 160 111111 ru 111111111 > 11111 |'i 11111111111 rll 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 u 22.00 22.20 22.40 22.60

31671.D SCAN508.M Tue Jan 22 08:37:27 2002 Page 9

NYC-WTC_000050036

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NYC-WTC_000050036Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD31585, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000049902

Laboratory report showing GCMS analysis of sample AD31585 including unknown compounds and surrogate recovery data.

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