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Document / 19 pages

GCMS analysis results, Feb 27 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for sample AE01136 testing unknown compounds and specific analytes on February 27, 2002.

NYC-WTC_000003444–000003462

Folder label: “GCMS X 1/20/02 A 2/25/02

Page image
Scanned page image, NYC-WTC_000003460
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB25\01136.D Vial: 3 Acq On : 25 Feb 2002 12:53 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *********************************************************** *** * * ** * * * Peak Number 11 N-perdeuteriobenzylideneani ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.11 ug/L 76734 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 1-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 1675 (22.283 min): 01136.D (-) m/z 192.00 100.00% 192

5000

96 82

m/z-> 0 — 44 74 118 TVPPIIWTTTTT 146 160 | TpTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l— 22.00 22.20 22.40 22.60 m/Z96.00 18.83% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 T TT 22.00 22.20 22.40 22.60 54 m/z 191.00 16.65% 110 30 0 ----- 1111'1' i' --H 1 94 ■ ■ 11 >1' i ■ ■ ■ ■ i ■ ■ । ■ i > mm 4 160 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192

22.00 22.20 22.40 22.60 5000 m/z 193.00 14.65%

144 177

0 T’T 1111' I'1" I'1'' 11 " ' 11 " ‘ 11" ' 11" ‘ I" 1' I'' " I'1' nnmmmm +p m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 22.00 22.20 22.40 22.60 77 151 m/z 146.10 12.18% 130 93 104 5000 119

177 0 "i ‘ ‘‘I v TITT 1’1 "ITT TT"IIEI"TUIO"I"IT‘‘7‘T "11" ————————— m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

01136.D HP022102.M Tue Feb 26 08:29:57 2002 Page 13 NYC-WTC_000003460

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NYC-WTC_000003460Source: NYC Law Department, mirrored locally

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