Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
NYC-WTC_000037635–000037654Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03508.D Vial: 4 Acq On : 8 Mar 2002 1:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 N-perdeuteriobenzylideneani ... Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.11 ug/L 84814 Phenanthrene-dl0 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 33 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 46 Abundance Scan 1675 (22.283 min): 03508.D (-) m/z 192.00 100.00% 192
5000
96 146 160 82 22.00 22.20 22.40 22.60 49 66 0 mmma +mmmmpmp — m/z 191.00 18.76% m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192
82 ----- 5000 22.00 22.20 22.40 22.60 54 110 m/z 96.00 17.41%
m/z—> 0 30 ‘ ■ i ■ ■" i1 ■ ■ i" “ i •1 1 94 — —mmpmm] 160 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 _________ I T-p-n-r-p-r * ’ I * ’ ’ ' I ' * 22.00 22.20 22.40 22.60 5000 m/z 146.00 15.24%
96 0 88 , WIB]unueWpgp , 139 152 TjTTT-rpTTp-rTTTp-rrrp rTTptTTphpnt Tr 165 176 _ miz—> 20 30 40 50 60 70 80 90 100 11Q 120 130 140 150 160 170 180 1«) 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... --A 159 192 22.00 22.20 22.40 22.60 m/z 193.10 14.41% 5000
144 177 — 0 , j pj , , । fi | j [ > I ) I J t . < i [ • : • . । M i t ] > i : i j ( i i t j > ! i . । >i!>.:»(iIii।r i • • i > • • ■ i • । 1 i ' ■ ■ ■ i' 1 miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
03508.D HP022102.M Fri Mar 15 10:08:52 2002 Page 15
NYC-WTC_000037653
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NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
1 shared topics · similarity 0.997
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Laboratory report listing concentrations of volatile organic compounds in sample AE03509 analyzed on March 19, 2002.
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