GCMS blank results for sample AE03508, March 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02MAR08\03508.D Vial: 4 Acq On : 8 Mar 2002 1:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Cyclopentasiloxane, decamet... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

12.54 0.08 ug/L 59189 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 >53 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 45 3 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 33 4 1,1,3,3,5,5,7,7-OCTAMETHYL-TETRA... 282 C8H26O3Si4 000000-00-0 33 Abundance Scan 812 (12.540 min): 03508.D (-) m/ z 73.00 100.00% '73

5000 267 355 —>-

45 12.20 12.40 12.60 12.80 193 251 | 0-• i •t • • • ।i ‘ ■ 1 I * । “I “ 1'i‘1 “ I TONTIWWIITLTLTT] T T" m/z 266.90 48.46% miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 ----- 5000 12.20 12.40 12.60 12.80 m/z 355.00 31.09% , , 191207 251 323339 0 IWBB3111111 UINI, 1113 . • • • । > 111 TII TWumnpmp mTT 1‘ miz-> 40 60 80 100 120 140 160 180 200 220 240 260280300320340360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ■ • i ■ » ■ ■ । • • i • • ■ • l • • • ‘ i 12.20 12.40 12.60 12.80 5000 267 m/z 356.00 14.42% 355 45 0 | | 193223 251 | 323339 I, TTTTTTTTTTTTT । i' i i i ] । I fi j i 1 I I । t I t i । :< i i । I i I i । i i I I | I I f i । 11 i : p i I f । : fT I ( i Ti i । i i i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #227689: Benzoic acid, 2-[(trimethylsilyl)oxy}-, trimethyl... TIITAIIT 1” ‘ 11I-1T T T 73 12.20 12.40 12.60 12.80 m/z 268.00 11.97%

50001 267

45 [ 135151 175 193 209 233249 [ 0IITITTema—dt-upuemanapaup • ■ i ■ 1 ■ 1 i ■ ■ l 1 ■ • ■ i • ■ ■ ■ i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80

03508.D HP022102.M Fri Mar 15 10:08:52 2002 Page 14

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