DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB26\02015.D Vial: 3 Acq On : 26 Feb 2002 11:57 am Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 1-amino-2-methyl -4-isopropy. .. Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 100077 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 2 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 47 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 45 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 45 Abundance Scan 1675 (22.283 min): 02015.D (-) m/z 192.00 100.00% 192

5000

82 96 146 16Q 22.00 22.20 22.40 22.60

/z-> 4970 O+ TII9nuuuamn]Tr H— i1 ■' ■ i1 ‘1111'1' I'1''' 11'' ''11 1 i111 <' 11 ■ 1 m/z 191.00 17.18% 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192

5000 22.00 22.20 22.40 22.60 144 177 m/z96.00 15.26%

m/z-> 01 111111 r ' ■11' 40 50 60 ‘ i " " r " 1 1 " " 11 1*T1111t 1 ■ । । • i111 ■ r ' 70 80 90 100 110 120 130 140 150 160 170 180 190 200 —pret... . I—— Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 77 151 * * i * > 1 ■ i 1 130 22.00 22.20 22.40 22.60 93 104 5000 m/z 193.00 12.23% 119

177 , ........ _........... O+ ■ । ■ > ■ ■ । ■ i " ■' i1 ■ "i ■ " 11 1111 -r-p-r 1’1 ’11’ ‘ | " I । ' C10—3/11 I ■ i r | 1, m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene I I 19/2 22.00 22.20 22.40 22.60 m/Z 146.10 11.37% 5000 1 96 155

m/z-> 0 21111011000000100011———— 40 50 60 70 80 88 J 139 152 90 100 110 120 130 140 150 160 170 180 190 200 ,| 176 4 ■ ■ i ■ ■ ' 1 i A । । । । । /1 n i

22.00 22.20 22.40 22.60

02015.D HP022102.M Wed Feb 27 08:34:26 2002 Page 14

NYC-WTC_000004562

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NYC-WTC_000004562Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999