DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02015.D Vial: 3 Acq On : 26 Feb 2002 11:57 am Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ****************************** * * * ************************************ Peak Number 11 2-CARBAMOYL-3-HYDROXY-4,5,5... Concentration Rank 13 R.T. EstConc Area Relative to ISTE R.T. 19.98 0.03 ug/L 22957 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIM... 186 C8H14N203 072700-98-2 7 2 Imidazole-2,4,5-d3 $$ IH-Imidazo ... 71 C3HD3N2 006745-43-3 4 3 IMIDAZOLE-1,4,5-D3 71 C3HD3N2 053716-57-7 3 4 2-Propenamide (CAS) $$ Acrylamid... 71 C3H5NO 000079-06-1 3 Abundance Scan 1471 (19.980 min): 02015. D (-) m/ z 71.00 100.00% 7h

5000 186 43

19.60 19.80 20.00 20.20 20.40 0 1‘1‘02111111011111117111117111 ‘17‘1‘"110101‘311-111111111‘1111‘12-1‘01‘011111111‘113 11"' m/ z 186.00 38.88% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #94657: 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIMETHYL-1-PYRROLINE... 71

5000 55 116 ■ i ' 1 ' ■ i ■ ' ' 1 i ■ ■ ' ■ i ■ 41 186 19.60 19.80 20.00 20.20 20.40 86 142 m/z 184.90 31.39%

0- " i" " r'1' I "1111 111121171117 " " r' ' r "' i' ■111" ' i" " r 1 " i " i''" i " ' ’ r ■ ‘' i " 111" miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #1085: lmidazole-2,4,5-d3 $$ 1 H-lmidazole-2,4,5-d3 (CAS) $... 71 19.60 19.80 20.00 20.20 20.40 5000 m/z 43.05 28.17% 43

16 30 V 0 "i1"1 [MH I, ________ p-rTrp-rTTp-rTrp-rTTp-rrTp-rrTp-TTTpT-rrp-rT-rp-rTTYTT^^ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #1084:1MIDAZOLE-1,4,5-D3 ' ' I ' ' i ■ ■ ■ ■ i 1 1 ' 1 1 1 71 19.60 19.80 20.00 20.20 20.40 m/z 49.00 3.35%

5000 44

0 Tp16 29 J 11"j 1 r " T > ■ ■ 11 ■ ■ > । > 11 > 11' 111. ।> 111 > 11 > 1111 ■ । । > ■. ■ । ।। । > 11 > > 11! < ■ 1 i ' ■ i ■ 1 ' ' i T1n rn/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 19.60 19.80 20.00 20.20 20.40

02015.D HP022102.M Wed Feb 27 08:34:26 2002 Page 13

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