GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
NYC-WTC_000010086–000010105Folder label: “GCMS X 1/23/02 A 2/21/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document . . Library Search Compound Report - -Data File : C: \MSDCHEM\1\5973N\02FEB21\01636.D Vial: 5 Acq On : 21 Feb 2002 6:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 2-CARBAMOYL-3-HYDROXY-4,5,5... Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T. 19.98 0.03 ug/L 22364 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIM. . . 186 C8H14N2O3 072700-98-2 7 2 Imidazole-2,4,5-d3 $$ lH-Imidazo... 71 C3HD3N2 006745-43-3 7 3 2-Propenamide (CAS) $$ Acrylamid. . . 71 C3H5NO 000079-06-1 3 4 IMIDAZOLE-1,4,5-D3 71 C3HD3N2 053716-57-7 3 Abundance Scan 1471 (19.980 min): 01636.D (-) m/ z 71.00 100.00% 71
5000 43 186 • J 1 * ‘ ' I ’ ‘ 19 60 19.80 20.00 20.20 20.40 0- ■ i ■1 ■ m/z 43.10 26.31% iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #94657:2-CARBAMOYL-3-HYDROXY-4,5,5-TRIMETHYL-1-PYRROLINE... 71
5000 55 116 1 114+414* r ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 41 186 19.60 19.80 20.00 20.20 20.40 86 142 m/z 186.10 23.25% 0- i-1‘‘“i “"i “"i' " r ■ “ i “ ’ 1117 ■ i ‘ ‘ "i"'' i' ■ 1’18 miz-> 10 2030405060 70 8090 100110120130140150 160170180190 Abundance #1085: Imidazole-2,4,5-d3 $$ 1H-Imidazole-2,4,5-d3 (CAS) $... 71 1 i 1 ■ ‘ ■ i ■ ' ■ ■ i ‘ ■ i ■ 19.60 19.80 20.00 20.20 20.40 5000 m/z 184.90 16.56% 43
m/z~> 16 0 TIItr 30 —+ 1....... V —871 ’13 jM k , । . . , , , . . , । । , i , , । , । . । । M J i j . CTTpn 1 PTTTTTs I | i : i 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 Abundance #1434:2-Propenamide (CAS) $$ Acrylamide $$ Propenamide $$... ‘ l ' ’ ’ ' I ’ ’ I * ‘ ‘ ’ I * * ’ ‘ | ’ 27 19.60 19.80 20.00 20.20 20.40 44 71 m/z 41.10 15.34% 55 5000
O-ppe A11eBaanat 'I T IT miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 19.60 19.80 20.00 20.20 20.40
01636.D HP022102.M Mon Feb 25 10:55:39 2002 Page 13
NYC-WTC_000010102
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NYC-WTC_000010106
GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010987
Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010927
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010066
GCMS laboratory results for sample AE01547 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011007
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02721 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010907
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010047
GCMS laboratory results for sample AE01511 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010887
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
2 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000009915
Administrative record from DEP Box 14 covering the period of January to February 2002 regarding World Trade Center environmental activities.
Filed in the same folder
NYC-WTC_000009916
GCMS blank sample results for target compounds showing non-detectable levels on February 25, 2002.
Filed in the same folder
NYC-WTC_000009918
Calibration data for GCMS analysis including response factors for various organic compounds recorded on February 21, 2002.
Filed in the same folder
NYC-WTC_000009937
Reference standard analysis report for GCMS testing verifying instrument performance with specific compound concentrations on February 25, 2002.
Filed in the same folder
NYC-WTC_000009941
Analytical results for sample AE01506 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
Filed in the same folder