DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02387.D Vial: 3 ’ Acq On : 27 Feb 2002 4:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 2-CARBAMOYL-3-HYDROXY-4,5,5... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 19.99 0.03 ug/L 17603 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIM... 186 C8H14N2O3 072700-98-2 5 2 Imidazole-2,4,5-d3 $$ IH-Imidazo. .. 71 C3HD3N2 006745-43-3 4 3 6-Methyl-7-hydroxy-8-adamantylme... 332 C18H24N2O2S 000000-00-0 4 4 2-ethylbutyl butyrate 172 C10H20O2 000000-00-0 4 Abundance Scan 1472 (19.991 min): 02387. D (-) m/ z 71.10 100.00% 71

43 149 5000 186 84 19.60 19.80 20.00 20.20 20.40 0- , , , , 1 , ,1. , , m/ Z 43.10 62.56% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #94657: 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIMETHYL-1-PYRROLINE... 7h

5000 55 116 41 186 19.60 19.80 20.00 20.20 20.40 86 142 m/ Z 149.00 60.65%

O- It11 11 ■ ■'11'11 ' i'' ' 11'' 1 r ■'11 1' i1'' 1 i1 1'' i1' " i'' ‘111 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #1086: lmidazole-2,4,5-d3 $$ 1 H-lmidazole-2,4,5-d3 (CAS) $... 71 43 19,60 19.80 20.00 20.20 20,40 5000 m/ z 186.00 35.19% A Oh '' 1111' 111 1’11’11111111171111111111111’1711111191 i11' ■ i ■' ■ ■ i111 ■ i ■1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #282793: 6-Methyl-7-hydroxy-8-adamantylmethylthiazolo[3,2-„. 1 I ' ' ' ' I 1 1 83 149 19.60 19.80 20.00 20.20 20.40 m/ Z 83.90 28.50% 93 135 5000 67 107 A W 127

1 49 .... ,1....... 0- " i " '11" " 11 " ' I'1 "11 J .... 1119, - ' i'' " i " '11 " ‘111 " ' i11 '' i ‘ 167 ' i ‘" i " " I'' ■ i ‘ ' m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 19.60 19.80 20.00 20.20 20.40

32387.D HP022102.M Thu Feb 28 08:47:17 2002 Page 13

NYC-WTC_000005062

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NYC-WTC_000005062Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999