Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02721 including surrogate recovery.
NYC-WTC_000011007–000011026Folder label: “GCMS X 2/5/02 A 2/28/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
*• Data File : C:\MSDCHEM\l\5973N\02FEB28\02721 .D Vial: 6 Acq On : 28 Feb 2002 6:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-CARBAMOYL-3-HYDROXY-4,5,5... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.
19.98 0.03 ug/L 17003 Ac enapht hene-d10 18.33
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-CARBAMOYL-3-HYDROXY-4, 5,5-TRIM... 186 C8H14N2O3 072700-98-2 9 2 Imidazole-2,4,5-d3 $$ lH-Imidazo... 71 C3HD3N2 006745-43-3 7 3 IMIDAZOLE-1,4,5-D3 71 C3HD3N2 053716-57-7 4 4 Imidazole-2,4,5-d3 $$ lH-Imidazo... 71 C3HD3N2 006745-43-3 4 Abundance Scan 1471 (19.980 min): 02721 .D (-) m/z 71.00 100.00% 71
5000 43 84 185 19.60 19.80 20.00 20.20 20.40 0- 11’01111001177717 »• I * ‘ “ I “«• I»> I ‘ ‘' I ‘ ‘ ‘ ‘ i" “ I “ “ I * “ ‘ I “ “ I “ 1 ‘ I ‘ ' I “ '' I ‘ “ I' • TJ-TT m/z 43.10 44.58% mfe-> 10 20 30 40 50 60 70 80 90 100 110120130140 150160 170180 190 Abundance #94657: 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIMETHYL-1-PYRROLINE... 71
5000- 55 116 * i 1 * ‘ ’ i ' ‘ i ’-r« ‘ • • i » 41 186 19 60 19.80 20.00 20.20 20.40 86 142 m/z 44.10 30.21%
miz—> 0 1 I‘ ’ • • I ’' ‘ *l ‘ ‘‘I ‘ • ’ I ‘ ‘ 1 1 “ * ’ * ' * I 1′1′301167144 ‘ I* ‘ ‘ 1+4411 • •||| * • • • | « H-p-rr
Abundance 10 2030405060 70 8090 100110120 130140 150160170180 190 #1086: Imidazole-2,4,5-d3 $$ 1 H-Imidazole-2,4,5-d3 (CAS) $... MNHRAMAwAN" 71 ‘ I’ * ‘ 4 I ' • ‘ I ’ ’ ‘ ' I ' ‘ • * i ’ 43 19.60 19.80 20.00 20.20 20.40 5000 rn/z 185.00 27.07%
0 • i • • • • t * * > * i •'1 • TTp-rTTp-rTT 1‘‘1111‘‘1—9/1t211D111232/11111//""£11-112T"21/1/2/1111111 m/z—> 10 2030405060 70 80a) 100110120130140 150160 170180 190 Abundance #1084: IMIDAZOLE-1,4,5-D3 ' I ' ■ ‘ ‘ I ' ‘ ' 1 I 1 ' ' ' I I 71 19.60 19.80 20.00 20.20 20.40 m/z 186.00 25.13% h 5000 44 16 29 I 0 mHHTphm i “ • ■ i ■ ■ ■ ■ 11 ■ ‘ ■ i •1 ■11 •' •11 ■ ■ “ i ■ ‘ ‘ ■ i ■ ■ “ i “ “ i “ ■ ■ i ■ ■ • ■ i ■ ■ ■ • i ■ • i * * * ‘ i * * • i ' m/z—> 10 20 30 40 50 60 70 80 90 100110120130140 150160170180 190 19.60 19.80 20.00 20.20 20.40
02721.D HP022102.M Fri Mar 01 10:07:53 2002 Page 11
NYC-WTC_000011021
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NYC-WTC_000010947
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010907
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010927
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010987
Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010887
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010066
GCMS laboratory results for sample AE01547 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010126
GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000010837
Administrative record from DEP Box 14 covering the period of February to March 2002 regarding World Trade Center environmental activities.
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NYC-WTC_000010838
Technical log recording laboratory parameters and counts for sample AE02713 processed in late February 2002.
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NYC-WTC_000010843
Laboratory report documenting a blank run for gas chromatography-mass spectrometry analysis of sample AE02713.
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NYC-WTC_000010862
Laboratory report documenting a reference standard run for gas chromatography-mass spectrometry analysis of sample AE02713.
Filed in the same folder
NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
Filed in the same folder