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← Document results/DEP Box 14/GCMS X 2/5/02 A 2/28/02
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GCMS analysis results for sample AE03075, March 5 2002

Machine-extracted title · confidence 50%

Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

NYC-WTC_000010927–000010946

Folder label: “GCMS X 2/5/02 A 2/28/02”

←Page 11 of 20→
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NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\l\5973N\02FEB28\02716.D Vial: 1 Acq On : 28 Feb 2002 2:40 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Imidazole-2,4,5-d3 $$ IH-Im... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 5.72 0.04 ug/L 13724 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Imidazole-2,4,5-d3 $$ lH-Imidazo. .. 71 C3HD3N2 006745-43-3 4 2 1-(Phenylsulfonyl)-4-hydroxybuta... 228 C10H12O4S 088703-48-4 4 3 Butane, 2,2-dimethyl- (CAS) $$ 2... 86 C6H14 000075-83-2 4 4 Azetidine, 2-methyl- (CAS) 71 C4H9N 019812-49-8 3 Abundance Scan 208 (5.722 min): 02716.D (-) m/ z 71.00 100.00% 43 71

5000 49 ■ ■ i ■ • ■ 1 I ■ ‘ 1 ■ i 1 ' ' ■ i ■ ■ ' ■ i 5.40 5.60 5.80 6.00 84 0 i....i1... i. •.* i. “ 2P9a—tmnnT m/z 43.10 87.61% nz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90

A Abundance #1086: Imidazole-2,4,5-d3 $$ 1 H-Imidazole-2,4,5-d3 (CAS) $... 71 43 5000 -A 5.40 ANMMM. 5.60 5.80 6.00 "I

40 m/ z 41.10 80.41% 0- I U I , |1 , 11. P l. .11... I... ■!... nfe-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #156179:1-(PhenylsulfonyI)-4-hydroxybutan-2-one$$2-Buta... 43 51 IF 77 5.40 5.60 5.80 6.00 5000 m/z 69.00 55.69% 39 55 0- ... t....jj.।।(।, T’ T ’ ’’’’’41’5 ■ i ■ ■111'1 ■ ■ i ■ ■ ■ miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4275: Butane, 2,2-dimethyl- (CAS) $$ 2,2-Dimethylbutane $... 43 517 71 5.40 5.60 5.80 6.00 ' ‘ m/z 45.10 34.54% 5000 27 5 15 53 mfz-> 0-mm m-r|-m-r m " ‘I"” i' tH .......... . ......... "l'“ ' I ” ‘ ‘ I 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 5.40 5.60 5.80 6.00 TI

02716.D HP022102.M Fri Mar 01 10:07:14 2002 Page 7

NYC-WTC_000010937

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

machine-extracted · confidence unavailable · Check page ↗

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