GCMS analysis results for sample AE03075, March 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB28\02716.D Vial: 1 Acq On : 28 Feb 2002 2:40 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Acetic acid, 3-[1,3]dioxola... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

5.95 0.29 ug/L 107145 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 38 2 3-(CYCLOHEX-3 ′ -EN-YL)PROPANOL $$ . . . 174 C8H14O4 015745-87-6 38 3 1-Propene-1-thiol 74 C3H6S 000925-89-3 9 4 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 9 Abundance Scan 228 (5.948 min): 02716.D (-) m/z 73.10 100.00% 73

5000 43 1’11* 5.60 5.806.00 6.20 ........ 1,1.55.... 1 ! 0-4 I 1t* ‘1**** J fl. 87 . .■» 1 1444 ‘18 1 “ । *1 ‘ ■ t । । ।। । । । ‘ । ‘ 11 ■ m/z 43.10 22.63% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-{1,3]dioxolan-2-yipropyl ester 73

5000 N W T !it 5.60 5.80 6.00 6.20 43 m/z 41.10 9.72% 27 87 55 113 174 0-TP ■ i ■ ■ "i1 • i• i * • । • —i' “ ■ i ■ ■ ■ ■ । । ■1' i ■ ■ ■■ i ■ ■ ’ ‘ i " i ■1 ■ ■ i ■1" i ■ A niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 -4 5.60 5.80 6.00 6.20 • * i '

5000 m/z 45.00 9.44% 43 27 55 , 87 113 174 0- mP i 11 “ 111 ■11 ‘ i ‘ 1uudtl———uu—TmmumDmmaag miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #2002:1-Propene-1-thiol T‘ Tr’II’ 73 5.60 5.80 6.00 6.20 m/z 71.00 6.68% 5000 43

1, 57 0 TIPWTTmatt '‘ i■ “ ■ i■ ■ ■ ■ i■ • • ■ i • ■ “ i■■■■i" '‘i'■• ■ i ‘‘ i “ ■ ■ i"i■ miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20 '

32716.D HP022102.M Fri Mar 01 10:07:14 2002 Page 8

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