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GCMS analysis results for sample AE03075, March 5 2002

Machine-extracted title · confidence 50%

Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

NYC-WTC_000010927–000010946

Folder label: “GCMS X 2/5/02 A 2/28/02”

←Page 13 of 20→
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB28\02716.D Vial: 1 Acq On : 28 Feb 2002 2:40 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Cyclopenten-l-one, 3-(ace... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.05 ug/L 25450 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Cyclopenten-l-one, 3-(acetyloxy)- 140 C7H803 018766-96-6 5 2 1,3,5,7-Tetraazatricyclo[3.3.1.1... 140 C6H12N4 000100-97-0 4 3 2-Methyl-3-methoxy-4H-pyran-4-one 140 C7H803 000000-00-0 4 4 Methenamine $$ 1,3,5,7-Tetraazaa... 140 C6H12N4 000100-97-0 3 Abundance Scan 886 (13.376 min): 02716.D (-) m/z 140.00 100.00% 1-0

5000

70 94 13.00 13.20 13.40 13.60 13.80 84 | m/z 69.90 13.24% Of 114124’1/11 ■ ■ i ‘ 1 • ■ i • ' ■ 1 i • ■ ' ■ i ‘ ■ i ' 1 1 1 i ■ • 1 ' I • ‘II mz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35384:2-Cyclopenten-1-one, 3-(acetyloxy)- 43

--- 5000 69 140 13.00 13.20 13.40 13.60 13.80 m/z 94.00 12.99% 97

niz-> op. 30I H 40 + 50 57

60 ■ ■ -T- ' ................. .. .. JI'i 11 70 80 90 100 110 120 130 112............ 140 TTT

Abundance #35202: 1,3,5,7-Tetraazatricyclo[3.3.1.1(3,7)decane (CAS)... 42 2 13.00 13.20 13.40 13.60 13.80 5000 m/z 44.00 8.88% 140

71 85 112 ob' ' ' 11 n/z-> 30I Abundance 40 50 60 70 80 90 100 110 120 #35380:2-MethyI-3-methoxy-4H-pyran-4-one 69 130 140

140 "II AAAAAAAANMAAMAMM 13.00 13.20 13.40 13.60 13.80 122 rn/z 83.90 2.68% 5000

82 110 97 op. ....................... ll....... ill, - ■ ■ i < ■ • ■ i ■ ■ ‘ ‘i■■■•। • ■ ■ ■ }4 II... "TF /z-> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

32716.D HP022102.M Fri Mar 01 10:07:14 2002 Page 9

NYC-WTC_000010939

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NYC-WTC_000010939Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

machine-extracted · confidence unavailable · Check page ↗

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