GCMS analysis report for sample AE01636, March 2002

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GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010086–000010105

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report . -Data File : C:\MSDCHEM\1\5973N\02FEB21\01636.D Vial: 5 Acq On : 21 Feb 2002 6:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propen-1-amine, N,N-di-2-... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T.

13.38 0.05 ug/L 31151 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propen-1-amine, N,N-di-2-prope... 137 C9H15N 000102-70-5 5 2 2-Methyl-3-methoxy-4H-pyran-4-one 140 C7H803 000000-00-0 4 3 Methenamine $$ 1,3,5,7-Tetraazaa... 140 C6H12N4 000100-97-0 3 4 2-Cyclopenten-l-one, 3-(acetyloxy)- 140 C7H803 018766-96-6 3 Abundance Scan 886 (13.376 min): 01636.D (-) m/z 140.00 100.00% 140

5000

70 84 94 108 13.00 13.20 13.40 13.60 13.80 44 | 0- ■ •I■■ • ■ i ■ • ■ ■ i ••■11'1111111'11'1111 —T -mm I ‘tt m/z 94.10 11.30% m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #32848: 2-Propen-1-amine, N,N-di-2-propenyl- (CAS) $$ Tria... 41 108 5000- 122 II— -m 96 13.00 13.20 13.40 13.60 13.80 67 137 m/z 70.00 10.75% 53 80

miz-> 0 10 ....... .. 1.. 20 30 40 50 60 70 TT H80 90 100 110 120 130 140 ■ i ■ ■ j_________H_________ 1 ’ ’ I k k 1 ’ I ’ ’ ‘ ’ I

Abundance #35380:2-Methyl-3-methoxy-4H-pyran-4-one 69 1-0 122 • i • > ...N........ 13.00 13.20 13.40 13.60 13.80 5000 m/z96.10 9.60% 82 110 97 oW || ■ ■ • । ■ 1111" IIi TII -n-p-r 1i. z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35198: Methenamine $$ 1,3,5,7-Tetraazaadamantane$$ 1,3.5... 42 13.00 13.20 13.40 13.60 13.80 rn/z 137.10 8.89% 5000 140

15 71 85 112 I 30 0 -n-p-m-p- " ' I " " i' ■ i ■ ■ ■ ■ i ■ ■ ■ ‘'i'‘ ■ 1 1 1 1,1 1 ■ p । । ■ p । । ■ |'I । । । p । । i p । ‘ T IB ■ t • ■ ‘ * i 1 ' 1 1 I * n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

01636.D HP022102.M Mon Feb 25 10:55:38 2002 Page 11

NYC-WTC_000010100

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GCMS analysis results for sample AE01637, March 2002 · Box DEP Box 14

NYC-WTC_000010106

GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

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